C₂₅H₂₆F₃N₇O₂

Base Information

Chemical Name:C₂₅H₂₆F₃N₇O₂
CAS No.:1314873-76-1
Molecular Formula:C₂₅H₂₆F₃N₇O₂
Molecular Weight:513.522
Hs Code.:

C<sub>25</sub>H<sub>26</sub>F<sub>3</sub>N<sub>7</sub>O<sub>2</sub>

Synonyms:C₂₅H₂₆F₃N₇O₂

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₂₅H₂₆F₃N₇O₂

Chemical Property:

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Technology Process of C₂₅H₂₆F₃N₇O₂

There total 8 articles about C₂₅H₂₆F₃N₇O₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 42.0%

: 1314873-89-6
3-[[3-methoxy-4-(4-methyl-1H-imidazol-1-yl)phenyl]amino]-5-[[3-(trifluoromethyl)phenyl]methyl]-1H-1,2,4-triazole-1-ethanamine

: 75-36-5
acetyl chloride

: 1314873-76-1
C₂₅H₂₆F₃N₇O₂

Guidance literature:: With triethylamine; In dichloromethane; at 20 ℃; for 1h;

Reference yield:

: 958245-17-5
1-(2-methoxy-4-nitrophenyl)-4-methyl-1H-imidazole

: 1314873-76-1
C₂₅H₂₆F₃N₇O₂

Guidance literature:: Multi-step reaction with 5 steps

1.1: hydrogen; thiophene / palladium 10% on activated carbon / methanol / 50 °C / Inert atmosphere

2.1: sodium nitrite; sulfuric acid / acetic acid / 0.5 h / 10 - 20 °C

2.2: 1 h / 20 °C

3.1: caesium carbonate; XPhos / tris-(dibenzylideneacetone)dipalladium⁽⁰⁾ / tert-butyl alcohol / 20 h / 100 °C / Inert atmosphere

4.1: hydrogenchloride; hydrogen / palladium 10% on activated carbon / isopropyl alcohol; methanol / 25 °C / Inert atmosphere

5.1: triethylamine / dichloromethane / 1 h / 20 °C

With thiophene; hydrogenchloride; sulfuric acid; hydrogen; caesium carbonate; triethylamine; sodium nitrite; XPhos; tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; palladium 10% on activated carbon; In methanol; dichloromethane; acetic acid; isopropyl alcohol; tert-butyl alcohol;

Reference yield:

: 454-16-0
1-fluoro-2-methoxy-4-nitrobenzene

: 1314873-76-1
C₂₅H₂₆F₃N₇O₂

Guidance literature:: Multi-step reaction with 6 steps

1.1: potassium carbonate / dimethyl sulfoxide / 16 h / 125 °C / Inert atmosphere

2.1: hydrogen; thiophene / palladium 10% on activated carbon / methanol / 50 °C / Inert atmosphere

3.1: sodium nitrite; sulfuric acid / acetic acid / 0.5 h / 10 - 20 °C

3.2: 1 h / 20 °C

4.1: caesium carbonate; XPhos / tris-(dibenzylideneacetone)dipalladium⁽⁰⁾ / tert-butyl alcohol / 20 h / 100 °C / Inert atmosphere

5.1: hydrogenchloride; hydrogen / palladium 10% on activated carbon / isopropyl alcohol; methanol / 25 °C / Inert atmosphere

6.1: triethylamine / dichloromethane / 1 h / 20 °C

With thiophene; hydrogenchloride; sulfuric acid; hydrogen; potassium carbonate; caesium carbonate; triethylamine; sodium nitrite; XPhos; tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; palladium 10% on activated carbon; In methanol; dichloromethane; acetic acid; dimethyl sulfoxide; isopropyl alcohol; tert-butyl alcohol;