3,5-bis-(dimethoxyphosphorylmethyl)benzoic acid diethoxyphosphorylmethylamide

Base Information

Chemical Name:3,5-bis-(dimethoxyphosphorylmethyl)benzoic acid diethoxyphosphorylmethylamide
CAS No.:367927-29-5
Molecular Formula:C₁₈H₃₂NO₁₀P₃
Molecular Weight:515.374
Hs Code.:

Synonyms:3,5-bis-(dimethoxyphosphorylmethyl)benzoic acid diethoxyphosphorylmethylamide

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Chemical Property of 3,5-bis-(dimethoxyphosphorylmethyl)benzoic acid diethoxyphosphorylmethylamide

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Technology Process of 3,5-bis-(dimethoxyphosphorylmethyl)benzoic acid diethoxyphosphorylmethylamide

There total 4 articles about 3,5-bis-(dimethoxyphosphorylmethyl)benzoic acid diethoxyphosphorylmethylamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 50917-72-1
aminomethylphosphonic acid diethyl ester

: 223449-19-2
5-carboxy-m-xylylenebisphosphonic acid tetramethyl ester

: 367927-29-5
3,5-bis-(dimethoxyphosphorylmethyl)benzoic acid diethoxyphosphorylmethylamide

Guidance literature:: With 4-methyl-morpholine; 2-propane phosphonic acid anhydride;
DOI:10.1021/ol025976q

Reference yield: 75.0%

: 50917-72-1
aminomethylphosphonic acid diethyl ester

: lithium 3,5-bis(dimethoxyphosphorylmethyl)benzoate

: 367927-29-5
3,5-bis-(dimethoxyphosphorylmethyl)benzoic acid diethoxyphosphorylmethylamide

Guidance literature:: With bis-(2-oxo-3-oxazolidinyl)phosphoryl chloride; N-ethyl-N,N-diisopropylamine; In ethanol; dichloromethane; at 20 ℃; for 72h;
DOI:10.1021/jo0156161

Reference yield:

: 25081-39-4
methyl 3,5-dimethylbenzoate

: 367927-29-5
3,5-bis-(dimethoxyphosphorylmethyl)benzoic acid diethoxyphosphorylmethylamide

Guidance literature:: Multi-step reaction with 3 steps

1.1: N-bromosuccinimide / AIBN / CCl₄ / 3 h / Heating

1.2: 35 percent / Heating

2.1: 89 percent / LiOH / methanol; H₂O / -10 - 20 °C

3.1: 75 percent / diisopropylethylamine; bis(2-oxo-3-oxazolidinyl)phosphinic acid chloride / CH₂Cl₂; ethanol / 72 h / 20 °C

With lithium hydroxide; N-Bromosuccinimide; bis-(2-oxo-3-oxazolidinyl)phosphoryl chloride; N-ethyl-N,N-diisopropylamine; 2,2'-azobis(isobutyronitrile); In methanol; tetrachloromethane; ethanol; dichloromethane; water; 1.2: Arbuzov reaction;
DOI:10.1021/jo0156161