3,5-bis(dimethylamino)benzyl phenylacetate

Base Information

Chemical Name:3,5-bis(dimethylamino)benzyl phenylacetate
CAS No.:1260507-94-5
Molecular Formula:C₁₉H₂₄N₂O₂
Molecular Weight:312.412
Hs Code.:

Synonyms:3,5-bis(dimethylamino)benzyl phenylacetate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 3,5-bis(dimethylamino)benzyl phenylacetate

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Technology Process of 3,5-bis(dimethylamino)benzyl phenylacetate

There total 2 articles about 3,5-bis(dimethylamino)benzyl phenylacetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

: 103-80-0
phenylacetyl chloride

: 198623-58-4
3,5-bis(dimethylamino)benzyl alcohol

: 1260507-94-5
3,5-bis(dimethylamino)benzyl phenylacetate

Guidance literature:: With triethylamine; In dichloromethane; at 20 ℃; Inert atmosphere;
DOI:10.1021/ol102606m

Reference yield:

: 1260507-92-3
ethyl 3,5-bis(dimethylamino)benzoate

: 1260507-94-5
3,5-bis(dimethylamino)benzyl phenylacetate

Guidance literature:: Multi-step reaction with 2 steps

1: lithium aluminium tetrahydride / tetrahydrofuran; mineral oil / 0 - 20 °C / Inert atmosphere

2: triethylamine / dichloromethane / 20 °C / Inert atmosphere

With lithium aluminium tetrahydride; triethylamine; In tetrahydrofuran; dichloromethane; mineral oil;
DOI:10.1021/ol102606m