p-nitrophenyl 2-O-(2,3,4-tri-O-acetyl-α-L-fucopyranosyl)-β-D-fucopyranoside

Base Information

Chemical Name:p-nitrophenyl 2-O-(2,3,4-tri-O-acetyl-α-L-fucopyranosyl)-β-D-fucopyranoside
CAS No.:84730-04-1
Molecular Formula:C₂₄H₃₁NO₁₄
Molecular Weight:557.508
Hs Code.:

Synonyms:p-nitrophenyl 2-O-(2,3,4-tri-O-acetyl-α-L-fucopyranosyl)-β-D-fucopyranoside

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Chemical Property of p-nitrophenyl 2-O-(2,3,4-tri-O-acetyl-α-L-fucopyranosyl)-β-D-fucopyranoside

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Technology Process of p-nitrophenyl 2-O-(2,3,4-tri-O-acetyl-α-L-fucopyranosyl)-β-D-fucopyranoside

There total 7 articles about p-nitrophenyl 2-O-(2,3,4-tri-O-acetyl-α-L-fucopyranosyl)-β-D-fucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 84730-02-9,84730-03-0
p-nitrophenyl 3,4-O-isopropylidene-2-O-(2,3,4-tri-O-acetyl-L-fucopyranosyl)-β-D-fucopyranoside

: 84730-05-2
p-nitrophenyl 2-O-(2,3,4-tri-O-acetyl-β-L-fucopyranosyl)-β-D-fucopyranoside

: 84730-04-1
p-nitrophenyl 2-O-(2,3,4-tri-O-acetyl-α-L-fucopyranosyl)-β-D-fucopyranoside

Guidance literature:: With water; trifluoroacetic acid; In ethyl acetate; for 1.5h; Ambient temperature;
DOI:10.1016/0008-6215(83)88286-X

Reference yield:

: 1226-39-7
p-nitrophenyl-β-D-fucopyranoside

: 84730-04-1
p-nitrophenyl 2-O-(2,3,4-tri-O-acetyl-α-L-fucopyranosyl)-β-D-fucopyranoside

Guidance literature:: Multi-step reaction with 3 steps

1: 95.4 percent / p-toluenesulfonic acid, triethylamine / dimethylformamide / 0.67 h / 80 °C

2: mercuric cyanide / acetonitrile / 3 h / Ambient temperature

3: 150 mg / trifluoroacetic acid, water / ethyl acetate; CHCl₃ / 1.5 h / Ambient temperature

With water; mercury(II) cyanide; toluene-4-sulfonic acid; triethylamine; trifluoroacetic acid; In chloroform; ethyl acetate; N,N-dimethyl-formamide; acetonitrile;
DOI:10.1016/0008-6215(83)88286-X

Reference yield:

: 84729-97-5
p-nitrophenyl 2,3,4-tri-O-acetyl-β-D-fucopyranoside

: 84730-04-1
p-nitrophenyl 2-O-(2,3,4-tri-O-acetyl-α-L-fucopyranosyl)-β-D-fucopyranoside

Guidance literature:: Multi-step reaction with 4 steps

1: 83.5 percent / 0.5 M sodium methoxide / methanol / 4 °C

2: 95.4 percent / p-toluenesulfonic acid, triethylamine / dimethylformamide / 0.67 h / 80 °C

3: mercuric cyanide / acetonitrile / 3 h / Ambient temperature

4: 150 mg / trifluoroacetic acid, water / ethyl acetate; CHCl₃ / 1.5 h / Ambient temperature

With water; sodium methylate; mercury(II) cyanide; toluene-4-sulfonic acid; triethylamine; trifluoroacetic acid; In methanol; chloroform; ethyl acetate; N,N-dimethyl-formamide; acetonitrile;
DOI:10.1016/0008-6215(83)88286-X