C₂₄H₂₉NO₃

Base Information

Chemical Name:C₂₄H₂₉NO₃
CAS No.:1394050-29-3
Molecular Formula:C₂₄H₂₉NO₃
Molecular Weight:379.499
Hs Code.:

C<sub>24</sub>H<sub>29</sub>NO<sub>3</sub>

Synonyms:C₂₄H₂₉NO₃

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Chemical Property of C₂₄H₂₉NO₃

Chemical Property:

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Technology Process of C₂₄H₂₉NO₃

There total 8 articles about C₂₄H₂₉NO₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 110-87-2
3,4-dihydro-2H-pyran

: 1394050-28-2
(3S,5R)-5-(biphenyl-4-yl-methyl)-3-(hydroxymethyl)-3-methylpyrrolidin-2-one

: 1394050-29-3
C₂₄H₂₉NO₃

Guidance literature:: 3,4-dihydro-2H-pyran; (3S,5R)-5-(biphenyl-4-yl-methyl)-3-(hydroxymethyl)-3-methylpyrrolidin-2-one; toluene-4-sulfonic acid; In dichloromethane; at 0 - 20 ℃; for 2h; Inert atmosphere;

With sodium hydrogencarbonate; In dichloromethane; water;

Reference yield:

: 128779-47-5
(2R)-3-(biphenyl-4-yl)-2-[(tert-butoxycarbonyl)amino]propanoic acid

: 1394050-29-3
C₂₄H₂₉NO₃

Guidance literature:: Multi-step reaction with 8 steps

1.1: dmap; dicyclohexyl-carbodiimide / dichloromethane / 9 h / -5 °C / Inert atmosphere

2.1: acetic acid / dichloromethane / 0.5 h / -5 °C / Inert atmosphere

2.2: 2 h / -5 °C / Inert atmosphere

3.1: potassium carbonate / N,N-dimethyl-formamide / 0 - 23 °C / Inert atmosphere

4.1: hydrogenchloride / cyclopentyl methyl ether / 24 h / 0 - 20 °C / Inert atmosphere

5.1: 2-methyltetrahydrofuran; cyclopentyl methyl ether / 20 °C / Inert atmosphere

6.1: 4-methyl-morpholine / tetrahydrofuran / 0.33 h / 0 - 5 °C / Inert atmosphere

7.1: sodium tetrahydroborate / water; tetrahydrofuran / 0.33 h / 0 °C / Inert atmosphere

8.1: toluene-4-sulfonic acid / dichloromethane / 2 h / 0 - 20 °C / Inert atmosphere

With 4-methyl-morpholine; hydrogenchloride; dmap; sodium tetrahydroborate; potassium carbonate; acetic acid; dicyclohexyl-carbodiimide; toluene-4-sulfonic acid; In tetrahydrofuran; 2-methyltetrahydrofuran; dichloromethane; cyclopentyl methyl ether; water; N,N-dimethyl-formamide;

Reference yield:

: 1383026-37-6
[(R)-1-biphenyl-4-ylmethyl-2-(2,2-dimethyl-4,6-dioxo-[1,3]dioxan-5-yl)-2-oxoethyl]carbamic acid t-butyl ester

: 1394050-29-3
C₂₄H₂₉NO₃

Guidance literature:: Multi-step reaction with 7 steps

1.1: acetic acid / dichloromethane / 0.5 h / -5 °C / Inert atmosphere

1.2: 2 h / -5 °C / Inert atmosphere

2.1: potassium carbonate / N,N-dimethyl-formamide / 0 - 23 °C / Inert atmosphere

3.1: hydrogenchloride / cyclopentyl methyl ether / 24 h / 0 - 20 °C / Inert atmosphere

4.1: 2-methyltetrahydrofuran; cyclopentyl methyl ether / 20 °C / Inert atmosphere

5.1: 4-methyl-morpholine / tetrahydrofuran / 0.33 h / 0 - 5 °C / Inert atmosphere

6.1: sodium tetrahydroborate / water; tetrahydrofuran / 0.33 h / 0 °C / Inert atmosphere

7.1: toluene-4-sulfonic acid / dichloromethane / 2 h / 0 - 20 °C / Inert atmosphere

With 4-methyl-morpholine; hydrogenchloride; sodium tetrahydroborate; potassium carbonate; acetic acid; toluene-4-sulfonic acid; In tetrahydrofuran; 2-methyltetrahydrofuran; dichloromethane; cyclopentyl methyl ether; water; N,N-dimethyl-formamide;