1-iodo-3-benzyloxy-4-(2',3',4',6'-tetra-O-benzyl-β-D-glucopyranosyloxy)benzene

Base Information

Chemical Name:1-iodo-3-benzyloxy-4-(2',3',4',6'-tetra-O-benzyl-β-D-glucopyranosyloxy)benzene
CAS No.:289471-95-0
Molecular Formula:C₄₇H₄₅IO₇
Molecular Weight:848.775
Hs Code.:

Synonyms:1-iodo-3-benzyloxy-4-(2',3',4',6'-tetra-O-benzyl-β-D-glucopyranosyloxy)benzene

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1-iodo-3-benzyloxy-4-(2',3',4',6'-tetra-O-benzyl-β-D-glucopyranosyloxy)benzene

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Technology Process of 1-iodo-3-benzyloxy-4-(2',3',4',6'-tetra-O-benzyl-β-D-glucopyranosyloxy)benzene

There total 2 articles about 1-iodo-3-benzyloxy-4-(2',3',4',6'-tetra-O-benzyl-β-D-glucopyranosyloxy)benzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 50.0%

: 74808-09-6
2,3,4,6-tetra-O-benzyl-α-D-glucopyranosyl trichloroacetimidate

: 289471-92-7
2-(benzyloxy)-4-iodophenol

: 289471-95-0
1-iodo-3-benzyloxy-4-(2',3',4',6'-tetra-O-benzyl-β-D-glucopyranosyloxy)benzene

Guidance literature:: With 4 A molecular sieve; boron trifluoride diethyl etherate; In dichloromethane; at -78 ℃; for 3.5h;
DOI:10.1016/S0040-4020(00)00325-2

Reference yield:

: 6272-38-4
O-benzylcatechol

: 289471-95-0
1-iodo-3-benzyloxy-4-(2',3',4',6'-tetra-O-benzyl-β-D-glucopyranosyloxy)benzene

Guidance literature:: Multi-step reaction with 2 steps

1: 58 percent / ICl / diethyl ether

2: 50 percent / BF₃*Et₂O; 4 Angstroem molecular sieves / CH₂Cl₂ / 3.5 h / -78 °C

With 4 A molecular sieve; boron trifluoride diethyl etherate; Iodine monochloride; In diethyl ether; dichloromethane; 1: Iodination / 2: Condensation;
DOI:10.1016/S0040-4020(00)00325-2

Reference yield:

: 1111-72-4
carbon dioxide

: 289471-95-0
1-iodo-3-benzyloxy-4-(2',3',4',6'-tetra-O-benzyl-β-D-glucopyranosyloxy)benzene

: 3-benzyloxy-4-(2',3',4',6'-tetra-O-benzyl-β-D-glucopyranosyloxy)benzoic acid

Guidance literature:: 1-iodo-3-benzyloxy-4-(2',3',4',6'-tetra-O-benzyl-β-D-glucopyranosyloxy)benzene; With n-butyllithium; In tetrahydrofuran; at -78 ℃; for 0.25h;

carbon dioxide; In tetrahydrofuran; at -78 ℃; for 0.25h; under 210 Torr;
DOI:10.1016/S0040-4020(00)00325-2