chlorodifluoromethyl phenethyl ketone

Base Information

Chemical Name:chlorodifluoromethyl phenethyl ketone
CAS No.:145299-85-0
Molecular Formula:C₁₀H₉ClF₂O
Molecular Weight:218.631
Hs Code.:

Synonyms:chlorodifluoromethyl phenethyl ketone

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Chemical Property of chlorodifluoromethyl phenethyl ketone

Chemical Property:

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Technology Process of chlorodifluoromethyl phenethyl ketone

There total 5 articles about chlorodifluoromethyl phenethyl ketone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: 3277-89-2
phenethylmagnesium bromide

: 1514-87-0
metyhyl chlorodifluoroacetate

: 145299-85-0
chlorodifluoromethyl phenethyl ketone

Guidance literature:: In diethyl ether; at -60 ℃; for 4h;
DOI:10.1016/S0022-1139(00)81174-4

Reference yield: 62.0%

: 383-62-0
ethyl 2-chloro-2,2-difluoroacetate

: 501-52-0
3-Phenylpropionic acid

: 145299-85-0
chlorodifluoromethyl phenethyl ketone

Guidance literature:: 3-Phenylpropionic acid; With lithium diisopropyl amide; In tetrahydrofuran; cyclohexane; at -20 - 20 ℃;

ethyl 2-chloro-2,2-difluoroacetate; In tetrahydrofuran; cyclohexane; at -65 ℃; for 0.25h;

With hydrogenchloride; In tetrahydrofuran; cyclohexane; water;
DOI:10.1021/jo801737c

Reference yield: 58.0%

: 1514-87-0
metyhyl chlorodifluoroacetate

: 103-63-9
1-phenyl-2-bromoethane

: 145299-85-0
chlorodifluoromethyl phenethyl ketone

Guidance literature:: 1-phenyl-2-bromoethane; With magnesium; In diethyl ether; at 20 ℃; for 1h;

metyhyl chlorodifluoroacetate; In diethyl ether; at -78 ℃; for 1h;
DOI:10.1016/j.jfluchem.2004.11.005