N-(tert-butoxycarbonyl)glycyl-N₁-[(1S)-2-azido-1-methylethyl]-N₂-(2,4-dimethoxybenzyl)glycinamide

Base Information

• Chemical Name: N-(tert-butoxycarbonyl)glycyl-N₁-[(1S)-2-azido-1-methylethyl]-N₂-(2,4-dimethoxybenzyl)glycinamide
• CAS No.: 1316672-54-4
• Molecular Formula: C₂₁H₃₂N₆O₆
• Molecular Weight: 464.522

Synonyms:N-(tert-butoxycarbonyl)glycyl-N₁-[(1S)-2-azido-1-methylethyl]-N₂-(2,4-dimethoxybenzyl)glycinamide

Chemical Property of N-(tert-butoxycarbonyl)glycyl-N₁-[(1S)-2-azido-1-methylethyl]-N₂-(2,4-dimethoxybenzyl)glycinamide

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Technology Process of N-(tert-butoxycarbonyl)glycyl-N₁-[(1S)-2-azido-1-methylethyl]-N₂-(2,4-dimethoxybenzyl)glycinamide

There total 1 articles about N-(tert-butoxycarbonyl)glycyl-N₁-[(1S)-2-azido-1-methylethyl]-N₂-(2,4-dimethoxybenzyl)glycinamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

BOC-glycine (4530-20-5) + formaldehyd (50-00-0,30525-89-4,61233-19-0) + (S)-1-azido-2-isocyanopropane (1223635-84-4) + 2,4-Dimethoxybenzylamine (20781-20-8) → N-(tert-butoxycarbonyl)glycyl-N1-[(1S)-2-azido-1-methylethyl]-N2-(2,4-dimethoxybenzyl)glycinamide (1316672-54-4)

Guidance literature:

In methanol; water; at 20 ℃; for 24h;

DOI:10.1039/c0ob01188f

Reference yield: 86.0%

N-(tert-butoxycarbonyl)glycyl-N1-[(1S)-2-azido-1-methylethyl]-N2-(2,4-dimethoxybenzyl)glycinamide (1316672-54-4) + methyl (3α,5β,7α,12α)-3,7,12-tris{[(prop-2-yn-1-yloxy)acetyl]oxy}cholan-24-oate (1316672-64-6) → C103H150N18O29 (1316672-94-2)

Guidance literature:

With copper(ll) sulfate pentahydrate; sodium L-ascorbate; In ethanol; water; at 40 ℃; for 12h;

DOI:10.1039/c0ob01188f

Reference yield: 80.0%

N-(tert-butoxycarbonyl)glycyl-N1-[(1S)-2-azido-1-methylethyl]-N2-(2,4-dimethoxybenzyl)glycinamide (1316672-54-4) + methyl (3α,5β,12α)-3,12-bis{[4-(prop-2-yn-1-yloxy)benzoyl]oxy}cholan-24-oate (1316672-60-2) → C87H118N12O20 (1316672-76-0)

Guidance literature:

With copper(ll) sulfate pentahydrate; sodium L-ascorbate; In dichloromethane; water; at 40 ℃; for 10h;

DOI:10.1039/c0ob01188f

upstream raw materials:

BOC-glycine

formaldehyd

(S)-1-azido-2-isocyanopropane

2,4-Dimethoxybenzylamine

Downstream raw materials:

C₇₄H₁₁₀N₁₂O₁₇

C₁₀₃H₁₅₀N₁₈O₂₉

C₈₇H₁₁₈N₁₂O₂₀

N₂-(tert-butoxycarbonyl)glycyl-N₂-(2,4-dimethoxybenzyl)-N₁-[(1S)-1-methyl-2-(4-[(1RS)-2,2,2-trifluoro-1-hydroxy-1-(methoxycarbonyl)ethyl]-1H-1,2,3-triazol-1-yl)ethyl]glycinamide

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