3-benzyl-1-(( 2-phenylselanyl)methyl)-3H-benzoimidazolium chloride

Base Information

• Chemical Name: 3-benzyl-1-(( 2-phenylselanyl)methyl)-3H-benzoimidazolium chloride
• CAS No.: 1616735-51-3
• Molecular Formula: C₂₁H₁₉N₂Se*Cl
• Molecular Weight: 413.808
• Mol file: 1616735-51-3.mol

Synonyms:3-benzyl-1-(( 2-phenylselanyl)methyl)-3H-benzoimidazolium chloride

Chemical Property of 3-benzyl-1-(( 2-phenylselanyl)methyl)-3H-benzoimidazolium chloride

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 3-benzyl-1-(( 2-phenylselanyl)methyl)-3H-benzoimidazolium chloride

There total 3 articles about 3-benzyl-1-(( 2-phenylselanyl)methyl)-3H-benzoimidazolium chloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

1-benzylbenzimidazole (4981-92-4) + chloromethyl phenylselenide (83442-19-7) → 3-benzyl-1-(( 2-phenylselanyl)methyl)-3H-benzoimidazolium chloride (1616735-51-3)

Guidance literature:

at 120 ℃; for 8h; Inert atmosphere; Schlenk technique;

DOI:10.1021/om500579r

Reference yield:

benzoimidazole (51-17-2,79351-71-6) → 3-benzyl-1-(( 2-phenylselanyl)methyl)-3H-benzoimidazolium chloride (1616735-51-3)

Guidance literature:

Multi-step reaction with 2 steps

1: potassium hydroxide; tetrabutylammomium bromide / tetrahydrofuran

2: 8 h / 120 °C / Inert atmosphere; Schlenk technique

With tetrabutylammomium bromide; potassium hydroxide; In tetrahydrofuran;

DOI:10.1021/om500579r

Reference yield:

benzyl bromide (100-39-0) → 3-benzyl-1-(( 2-phenylselanyl)methyl)-3H-benzoimidazolium chloride (1616735-51-3)

Guidance literature:

Multi-step reaction with 2 steps

1: potassium hydroxide; tetrabutylammomium bromide / tetrahydrofuran

2: 8 h / 120 °C / Inert atmosphere; Schlenk technique

With tetrabutylammomium bromide; potassium hydroxide; In tetrahydrofuran;

DOI:10.1021/om500579r

upstream raw materials:

1-benzylbenzimidazole

chloromethyl phenylselenide

benzyl bromide

benzoimidazole

Downstream raw materials:

1-benzyl-3-phenylselenomethyl-1,3-dihydrobenzoimidazole-2-selenone

1-benzyl-3-phenylselenomethyl-1,3-dihydrobenzoimidazole-2-thione