2,9-Dicyclohexyl-5,12-bis-(3-methyl-hex-1-ynyl)-anthra[2,1,9-def;6,5,10-d'e'f']diisoquinoline-1,3,8,10-tetraone

Base Information

Chemical Name:2,9-Dicyclohexyl-5,12-bis-(3-methyl-hex-1-ynyl)-anthra[2,1,9-def;6,5,10-d'e'f']diisoquinoline-1,3,8,10-tetraone
CAS No.:209111-79-5
Molecular Formula:C₅₀H₅₀N₂O₄
Molecular Weight:742.958
Hs Code.:

Synonyms:2,9-Dicyclohexyl-5,12-bis-(3-methyl-hex-1-ynyl)-anthra[2,1,9-def;6,5,10-d'e'f']diisoquinoline-1,3,8,10-tetraone

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Chemical Property of 2,9-Dicyclohexyl-5,12-bis-(3-methyl-hex-1-ynyl)-anthra[2,1,9-def;6,5,10-d'e'f']diisoquinoline-1,3,8,10-tetraone

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Technology Process of 2,9-Dicyclohexyl-5,12-bis-(3-methyl-hex-1-ynyl)-anthra[2,1,9-def;6,5,10-d'e'f']diisoquinoline-1,3,8,10-tetraone

There total 4 articles about 2,9-Dicyclohexyl-5,12-bis-(3-methyl-hex-1-ynyl)-anthra[2,1,9-def;6,5,10-d'e'f']diisoquinoline-1,3,8,10-tetraone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 40276-93-5
3-methylhex-1-yne

: 191997-95-2
N,N'-dicyclohexyl-1,7-dibromoperylene-3,4:9,10-tetracarboxylic dianhydride

: 209111-79-5
2,9-Dicyclohexyl-5,12-bis-(3-methyl-hex-1-ynyl)-anthra[2,1,9-def;6,5,10-d'e'f']diisoquinoline-1,3,8,10-tetraone

Guidance literature:: With triethylamine; copper(l) iodide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In tetrahydrofuran; at 80 ℃; for 14h; Yield given;
DOI:10.1002/(SICI)1521-3773(19980605)37:10<1434::AID-ANIE1434>3.0.CO;2-P

Reference yield:

: 108-91-8,157973-60-9
cyclohexylamine

: 209111-79-5
2,9-Dicyclohexyl-5,12-bis-(3-methyl-hex-1-ynyl)-anthra[2,1,9-def;6,5,10-d'e'f']diisoquinoline-1,3,8,10-tetraone

Guidance literature:: Multi-step reaction with 2 steps

1: CH₃COOH / various solvent(s) / 8 h / 85 °C

2: Et₃N / Pd(PPh₃)4, CuI / tetrahydrofuran / 14 h / 80 °C

With acetic acid; triethylamine; copper(l) iodide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In tetrahydrofuran;
DOI:10.1002/(SICI)1521-3773(19980605)37:10<1434::AID-ANIE1434>3.0.CO;2-P

Reference yield:

: 128-69-8
perylene-3,4,9,10-tetracarboxylic acid 3,4:9,10-dianhydride

: 209111-79-5
2,9-Dicyclohexyl-5,12-bis-(3-methyl-hex-1-ynyl)-anthra[2,1,9-def;6,5,10-d'e'f']diisoquinoline-1,3,8,10-tetraone

Guidance literature:: Multi-step reaction with 3 steps

1: 95 percent / Br₂, H₂SO₄ / 12 h / 40 °C

2: CH₃COOH / various solvent(s) / 8 h / 85 °C

3: Et₃N / Pd(PPh₃)4, CuI / tetrahydrofuran / 14 h / 80 °C

With sulfuric acid; bromine; acetic acid; triethylamine; copper(l) iodide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In tetrahydrofuran;
DOI:10.1002/(SICI)1521-3773(19980605)37:10<1434::AID-ANIE1434>3.0.CO;2-P