Unii-HJ1pbz6dve

Base Information

• Chemical Name: Unii-HJ1pbz6dve
• CAS No.: 2973-18-4
• Molecular Formula: C₁₃H₈Cl₂N₂O₄
• Molecular Weight: 327.124
• DSSTox Substance ID: DTXSID201267508
• Mol file: 2973-18-4.mol

Synonyms:NSC 77614;BRN 2168611;UNII-HJ1PBZ6DVE;DTXSID201267508;LS-89983;1,1'-Methylenebis[4-chloro-3-nitrobenzene];2973-18-4

Chemical Property of Unii-HJ1pbz6dve

Chemical Property:

• XLogP3: 4.8
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 4
• Rotatable Bond Count: 2
• Exact Mass: 325.9861121
• Heavy Atom Count: 21
• Complexity: 363

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

• Canonical SMILES: C1=CC(=C(C=C1CC2=CC(=C(C=C2)Cl)[N+](=O)[O-])[N+](=O)[O-])Cl

Technology Process of Unii-HJ1pbz6dve

There total 7 articles about Unii-HJ1pbz6dve which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2-Chloronitrobenzene (88-73-3) → 4,4'-Dichloro-3,3'-dinitrodiphenylmethane (2973-18-4) + 1-chloro-4-(chloromethyl)-2-nitrobenzene (57403-35-7)

Guidance literature:

With hydrogenchloride; formaldehyd; sulfuric acid; at 85 ℃;

Reference yield:

formaldehyd (50-00-0,30525-89-4,61233-19-0) + 2-Chloronitrobenzene (88-73-3) → 4,4'-Dichloro-3,3'-dinitrodiphenylmethane (2973-18-4) + 1-chloro-4-(chloromethyl)-2-nitrobenzene (57403-35-7)

Guidance literature:

With hydrogenchloride; sulfuric acid; at 85 ℃;

Reference yield:

chlorobenzene (108-90-7) → 4,4'-Dichloro-3,3'-dinitrodiphenylmethane (2973-18-4)

Guidance literature:

Multi-step reaction with 2 steps

1: concentrated sulfuric acid

2: nitric acid (D: 1.42)

With sulfuric acid; nitric acid;

upstream raw materials:

4,4'-dichlorodiphenylmethane

formaldehyd

2-Chloronitrobenzene

nitric acid

Downstream raw materials:

4,4'-dichloro-3,3'-dinitrobenzophenone

bis(4-chloro-3-isocyanatophenyl)methane

3,3'-dinitro-4,4'-diaminodiphenylmethane