TRIPHENYLANTIMONY(V) DIBENZOATE 97

Base Information

Chemical Name:TRIPHENYLANTIMONY(V) DIBENZOATE 97
CAS No.:57997-56-5
Molecular Formula:(C6H5)3Sb(O2CC6H5)2
Molecular Weight:595.298
Hs Code.:
European Community (EC) Number:684-536-6
DSSTox Substance ID:DTXSID60586830
Wikidata:Q82479039
Mol file:57997-56-5.mol

Synonyms:TRIPHENYLANTIMONY(V) DIBENZOATE 97;triphenylantimony(v) dibenzoate

Suppliers and Price of TRIPHENYLANTIMONY(V) DIBENZOATE 97

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 3 raw suppliers

Chemical Property of TRIPHENYLANTIMONY(V) DIBENZOATE 97

Chemical Property:

Melting Point:174-179 °C(lit.)
PSA：80.26000
LogP:4.89810
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:4
Rotatable Bond Count:9
Exact Mass:594.07910
Heavy Atom Count:37
Complexity:666

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:Xn,N
Statements: 20/22-51/53
Safety Statements: 61

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1=CC=C(C=C1)C(=O)O[Sb](C2=CC=CC=C2)(C3=CC=CC=C3)(C4=CC=CC=C4)OC(=O)C5=CC=CC=C5

Technology Process of TRIPHENYLANTIMONY(V) DIBENZOATE 97

There total 9 articles about TRIPHENYLANTIMONY(V) DIBENZOATE 97 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 553-54-8
lithium benzoate

: 603-36-1
triphenylantimony

: 57997-56-5
triphenylantimony bisbenzoate

Guidance literature:: In acetonitrile; Electrolysis; N2 atmosphere, ambient temp.; constant current electrolysis (Pt plate and wire electrodes); extraction (ethyl acetate), washing of extracts (water, brine), drying (MgSO4), solvent removal, recrystn. (ethanol); elem. anal.;
DOI:10.1016/S0013-4686(97)85470-9

Reference yield: 85.0%

: 532-32-1
sodium benzoate

: 594-31-0,34716-91-1,20265-29-6
triphenylantimony dichloride

: 57997-56-5
triphenylantimony bisbenzoate

Guidance literature:: In toluene; byproducts: NaCl; evacuated glass tubes, heating (6 h, 90-100°C); soln. filtration, isopropanol addn. to filtrate, pptn. on cooling;

Reference yield: 75.0%

: 532-32-1
sodium benzoate

: 671235-22-6
tri-p-tolylantimony bis(2,3-dimethylbenzenesulfonate)

: 57997-56-5
triphenylantimony dibenzoate

Guidance literature:: In toluene; byproducts: sodium 2,4-dimethylbenzenesulfonate; a mixt. of Sb-contg. compd. and sodium benzoate in toluene was heated for 6 h at 90°C; the crystals were filtered off; the toluene was removed;
DOI:10.1023/A:1024945617228