phenyl 3,5-di-O-benzyl-2-O-2-naphthylmethyl-1-thio-α-L-arabinofuranoside

Base Information

Chemical Name:phenyl 3,5-di-O-benzyl-2-O-2-naphthylmethyl-1-thio-α-L-arabinofuranoside
CAS No.:1448452-71-8
Molecular Formula:C₃₆H₃₄O₄S
Molecular Weight:562.73
Hs Code.:

Synonyms:phenyl 3,5-di-O-benzyl-2-O-2-naphthylmethyl-1-thio-α-L-arabinofuranoside

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of phenyl 3,5-di-O-benzyl-2-O-2-naphthylmethyl-1-thio-α-L-arabinofuranoside

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Technology Process of phenyl 3,5-di-O-benzyl-2-O-2-naphthylmethyl-1-thio-α-L-arabinofuranoside

There total 4 articles about phenyl 3,5-di-O-benzyl-2-O-2-naphthylmethyl-1-thio-α-L-arabinofuranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 79.0%

: 1448452-72-9
phenyl 3,5-di-O-benzyl-2-O-(2-naphthyl)methyl-1-thio-α-Larabinofuranoside

: 100-39-0
benzyl bromide

: 1448452-71-8
phenyl 3,5-di-O-benzyl-2-O-2-naphthylmethyl-1-thio-α-L-arabinofuranoside

Guidance literature:: With sodium hydride; In N,N-dimethyl-formamide; mineral oil; at 0 ℃; for 2h; Inert atmosphere;
DOI:10.1039/c3ob40958a

Reference yield:

: 913060-78-3
phenyl 3,5-O-(di-tert-butylsilanediyl)-1-thio-α-L-arabinofuranoside

: 1448452-71-8
phenyl 3,5-di-O-benzyl-2-O-2-naphthylmethyl-1-thio-α-L-arabinofuranoside

Guidance literature:: Multi-step reaction with 3 steps

1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 3 h / 0 °C / Inert atmosphere

2: pyridine; pyridine hydrogenfluoride / dichloromethane / 2 h / 0 °C / Inert atmosphere

3: sodium hydride / N,N-dimethyl-formamide; mineral oil / 2 h / 0 °C / Inert atmosphere

With pyridine; sodium hydride; pyridine hydrogenfluoride; In dichloromethane; N,N-dimethyl-formamide; mineral oil;
DOI:10.1039/c3ob40958a

Reference yield:

: 1448452-68-3
phenyl 3,5-O-(di-tert-butylsilanediyl)-2-O-2-naphthylmethyl-1-thio-α-L-arabinofuranoside

: 1448452-71-8
phenyl 3,5-di-O-benzyl-2-O-2-naphthylmethyl-1-thio-α-L-arabinofuranoside

Guidance literature:: Multi-step reaction with 2 steps

1: pyridine; pyridine hydrogenfluoride / dichloromethane / 2 h / 0 °C / Inert atmosphere

2: sodium hydride / N,N-dimethyl-formamide; mineral oil / 2 h / 0 °C / Inert atmosphere

With pyridine; sodium hydride; pyridine hydrogenfluoride; In dichloromethane; N,N-dimethyl-formamide; mineral oil;
DOI:10.1039/c3ob40958a