carbonic acid {[2-(tert-butoxycarbonyl-methyl-amino)-ethyl]-methyl-carbamoyl}-[4-({2-[(3-hydroxy-3-methyl-5-oxo-hexyloxycarbonyl)-methyl-amino]-ethyl}-methyl-carbamoyloxy)-phenyl]-methyl ester 4-nitro-phenyl ester

Base Information

Chemical Name:carbonic acid {[2-(tert-butoxycarbonyl-methyl-amino)-ethyl]-methyl-carbamoyl}-[4-({2-[(3-hydroxy-3-methyl-5-oxo-hexyloxycarbonyl)-methyl-amino]-ethyl}-methyl-carbamoyloxy)-phenyl]-methyl ester 4-nitro-phenyl ester
CAS No.:560101-08-8
Molecular Formula:C₃₇H₅₁N₅O₁₄
Molecular Weight:789.837
Hs Code.:

carbonic acid {[2-(<i>tert</i>-butoxycarbonyl-methyl-amino)-ethyl]-methyl-carbamoyl}-[4-({2-[(3-hydroxy-3-methyl-5-oxo-hexyloxycarbonyl)-methyl-amino]-ethyl}-methyl-carbamoyloxy)-phenyl]-methyl ester 4-nitro-phenyl ester

Synonyms:carbonic acid {[2-(tert-butoxycarbonyl-methyl-amino)-ethyl]-methyl-carbamoyl}-[4-({2-[(3-hydroxy-3-methyl-5-oxo-hexyloxycarbonyl)-methyl-amino]-ethyl}-methyl-carbamoyloxy)-phenyl]-methyl ester 4-nitro-phenyl ester

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Chemical Property of carbonic acid {[2-(tert-butoxycarbonyl-methyl-amino)-ethyl]-methyl-carbamoyl}-[4-({2-[(3-hydroxy-3-methyl-5-oxo-hexyloxycarbonyl)-methyl-amino]-ethyl}-methyl-carbamoyloxy)-phenyl]-methyl ester 4-nitro-phenyl ester

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Technology Process of carbonic acid {[2-(tert-butoxycarbonyl-methyl-amino)-ethyl]-methyl-carbamoyl}-[4-({2-[(3-hydroxy-3-methyl-5-oxo-hexyloxycarbonyl)-methyl-amino]-ethyl}-methyl-carbamoyloxy)-phenyl]-methyl ester 4-nitro-phenyl ester

There total 4 articles about carbonic acid {[2-(tert-butoxycarbonyl-methyl-amino)-ethyl]-methyl-carbamoyl}-[4-({2-[(3-hydroxy-3-methyl-5-oxo-hexyloxycarbonyl)-methyl-amino]-ethyl}-methyl-carbamoyloxy)-phenyl]-methyl ester 4-nitro-phenyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

: 7693-46-1
4-Nitrophenyl chloroformate

: 560101-06-6
(2-{[4-({[2-(tert-butoxycarbonyl-methyl-amino)-ethyl]-methyl-carbamoyl}-hydroxy-methyl)-phenoxycarbonyl]-methyl-amino}-ethyl)-methyl-carbamic acid 3-hydroxy-3-methyl-5-oxo-hexyl ester

: 560101-08-8
carbonic acid {[2-(tert-butoxycarbonyl-methyl-amino)-ethyl]-methyl-carbamoyl}-[4-({2-[(3-hydroxy-3-methyl-5-oxo-hexyloxycarbonyl)-methyl-amino]-ethyl}-methyl-carbamoyloxy)-phenyl]-methyl ester 4-nitro-phenyl ester

Guidance literature:: With triethylamine;
DOI:10.1002/anie.200390108

Reference yield:

: 1198-84-1
4-hydroxymandelic acid

: 560101-08-8
carbonic acid {[2-(tert-butoxycarbonyl-methyl-amino)-ethyl]-methyl-carbamoyl}-[4-({2-[(3-hydroxy-3-methyl-5-oxo-hexyloxycarbonyl)-methyl-amino]-ethyl}-methyl-carbamoyloxy)-phenyl]-methyl ester 4-nitro-phenyl ester

Guidance literature:: Multi-step reaction with 4 steps

1: 49 percent / 1-[3-(dimethylamino)propyl]-3-ethylcarbodiimide; 1-hydroxybenzotriazole

2: 90 percent / Et₃N

3: 72 percent / Et₃N

With benzotriazol-1-ol; N-(3-dimethylaminopropyl)-N-ethylcarbodiimide; triethylamine;
DOI:10.1002/anie.200390108

Reference yield:

: 177587-81-4
bis(1,1-dimethylethyl) [1,2-ethylenediamine]-1,1'-dicarboxylate

: 560101-08-8
carbonic acid {[2-(tert-butoxycarbonyl-methyl-amino)-ethyl]-methyl-carbamoyl}-[4-({2-[(3-hydroxy-3-methyl-5-oxo-hexyloxycarbonyl)-methyl-amino]-ethyl}-methyl-carbamoyloxy)-phenyl]-methyl ester 4-nitro-phenyl ester

Guidance literature:: Multi-step reaction with 4 steps

1: 49 percent / 1-[3-(dimethylamino)propyl]-3-ethylcarbodiimide; 1-hydroxybenzotriazole

2: 90 percent / Et₃N

3: 72 percent / Et₃N

With benzotriazol-1-ol; N-(3-dimethylaminopropyl)-N-ethylcarbodiimide; triethylamine;
DOI:10.1002/anie.200390108