(2,4,6-tris[bis(trimethylsilyl)methyl]phenyl)hydroxy(mesityl)(methylthio)germane

Base Information

Chemical Name:(2,4,6-tris[bis(trimethylsilyl)methyl]phenyl)hydroxy(mesityl)(methylthio)germane
CAS No.:162088-82-6
Molecular Formula:C₃₇H₇₄GeOSSi₆
Molecular Weight:808.163
Hs Code.:

Synonyms:(2,4,6-tris[bis(trimethylsilyl)methyl]phenyl)hydroxy(mesityl)(methylthio)germane

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (2,4,6-tris[bis(trimethylsilyl)methyl]phenyl)hydroxy(mesityl)(methylthio)germane

Chemical Property:

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Technology Process of (2,4,6-tris[bis(trimethylsilyl)methyl]phenyl)hydroxy(mesityl)(methylthio)germane

There total 8 articles about (2,4,6-tris[bis(trimethylsilyl)methyl]phenyl)hydroxy(mesityl)(methylthio)germane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 135139-74-1
[2,4,6-tris[bis(trimethylsilyl)methyl]phenyl](hyroxy)(mercapto)(mesityl)germane

: 74-88-4
methyl iodide

: 162088-82-6
(2,4,6-tris[bis(trimethylsilyl)methyl]phenyl)hydroxy(mesityl)(methylthio)germane

Guidance literature:: With NaBH₄; In tetrahydrofuran; Ar-atmosphere; room temp. (3 h); filtering, evapn. (reduced pressure), chromy. (SiO2, hexane / CH2Cl2 = 3: 1); elem. anal.;
DOI:10.1021/om00002a055

Reference yield:

: 2633-66-1
2-mesitylmagnesium bromide

: 162088-82-6
(2,4,6-tris[bis(trimethylsilyl)methyl]phenyl)hydroxy(mesityl)(methylthio)germane

Guidance literature:: Multi-step reaction with 5 steps

1: t-BuLi; NH₄Cl / tetrahydrofuran; pentane

2: t-BuLi / tetrahydrofuran; pentane

3: benzene

4: hexamethylphosphorous triamide / tetrahydrofuran

5: NaBH₄ / tetrahydrofuran

With t-BuLi; NH₄Cl; hexamethylphosphorous triamide; NaBH₄; In tetrahydrofuran; pentane; benzene;
DOI:10.1021/om00002a055

Reference yield:

: 115160-05-9
1-bromo-2,4,6-tris[bis(trimethylsilyl)methyl]benzene

: 162088-82-6
(2,4,6-tris[bis(trimethylsilyl)methyl]phenyl)hydroxy(mesityl)(methylthio)germane

Guidance literature:: Multi-step reaction with 5 steps

1: t-BuLi; NH₄Cl / tetrahydrofuran; pentane

2: t-BuLi / tetrahydrofuran; pentane

3: benzene

4: hexamethylphosphorous triamide / tetrahydrofuran

5: NaBH₄ / tetrahydrofuran

With t-BuLi; NH₄Cl; hexamethylphosphorous triamide; NaBH₄; In tetrahydrofuran; pentane; benzene;
DOI:10.1021/om00002a055