(-)-(1S,2R,5S)-1-Chloroacetoxy-5-methyl-2-(1-methyl-1-phenylethyl)cyclohexane

Base Information

Chemical Name:(-)-(1S,2R,5S)-1-Chloroacetoxy-5-methyl-2-(1-methyl-1-phenylethyl)cyclohexane
CAS No.:122449-89-2
Molecular Formula:C₁₈H₂₅ClO₂
Molecular Weight:308.848
Hs Code.:

Synonyms:(-)-(1S,2R,5S)-1-Chloroacetoxy-5-methyl-2-(1-methyl-1-phenylethyl)cyclohexane

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (-)-(1S,2R,5S)-1-Chloroacetoxy-5-methyl-2-(1-methyl-1-phenylethyl)cyclohexane

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Technology Process of (-)-(1S,2R,5S)-1-Chloroacetoxy-5-methyl-2-(1-methyl-1-phenylethyl)cyclohexane

There total 2 articles about (-)-(1S,2R,5S)-1-Chloroacetoxy-5-methyl-2-(1-methyl-1-phenylethyl)cyclohexane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 57707-91-2
(1S,2R,5S)-8-(+)-phenylmenthol

: 79-04-9
chloroacetyl chloride

: 122449-89-2
(-)-(1S,2R,5S)-1-Chloroacetoxy-5-methyl-2-(1-methyl-1-phenylethyl)cyclohexane

Guidance literature:: With N,N-diethylaniline; In diethyl ether; Heating;
DOI:10.1016/S0040-4039(00)94713-0

Reference yield:

: (S)-5-Methyl-2-(1-methyl-1-phenyl-ethyl)-cyclohexanol

: 79-11-8
chloroacetic acid

: 122449-89-2
(-)-(1S,2R,5S)-1-Chloroacetoxy-5-methyl-2-(1-methyl-1-phenylethyl)cyclohexane

: 122427-41-2
(+)-(1R,2S,5S)-1-Chloroacetoxy-5-methyl-2-(1-methyl-1-phenylethyl)cyclohexane

Guidance literature:: With oxalyl dichloride; Yield given. Multistep reaction. Yields of byproduct given; 1.) DMF, CH₂Cl₂, -15 deg C, 30 min, then room temp., 1 h, 2.) CH₂Cl₂, room temp., 12 h;
DOI:10.1055/s-1988-27724