thyl (E)-4-Bromo-3-chlorocinnamate

Base Information

Chemical Name:thyl (E)-4-Bromo-3-chlorocinnamate
CAS No.:1308279-93-7
Molecular Formula:C₁₁H₁₀BrClO₂
Molecular Weight:289.556
Hs Code.:

Synonyms:thyl (E)-4-Bromo-3-chlorocinnamate

Suppliers and Price of thyl (E)-4-Bromo-3-chlorocinnamate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Total 1 raw suppliers

Chemical Property of thyl (E)-4-Bromo-3-chlorocinnamate

Chemical Property:

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

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Technology Process of thyl (E)-4-Bromo-3-chlorocinnamate

There total 2 articles about thyl (E)-4-Bromo-3-chlorocinnamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 57418-97-0
4‐bromo‐3‐chlorobenzonitrile

: 1308279-93-7
thyl (E)-4-Bromo-3-chlorocinnamate

Guidance literature:: Multi-step reaction with 2 steps

1: diisobutylaluminium hydride / dichloromethane; toluene / -78 - 20 °C

2: toluene / 17 h / Reflux

With diisobutylaluminium hydride; In dichloromethane; toluene; 2: Wittig reaction;
DOI:10.1021/jm200051z

Reference yield:

: 21803-75-8
4-amino-3-chlorobenzonitrile

: 1308279-93-7
thyl (E)-4-Bromo-3-chlorocinnamate

Guidance literature:: Multi-step reaction with 3 steps

1: tert.-butylnitrite; copper(ll) bromide / acetonitrile / 0 - 20 °C

2: diisobutylaluminium hydride / dichloromethane; toluene / -78 - 20 °C

3: toluene / 17 h / Reflux

With tert.-butylnitrite; diisobutylaluminium hydride; copper(ll) bromide; In dichloromethane; toluene; acetonitrile; 3: Wittig reaction;
DOI:10.1021/jm200051z