[2,2']bipyridinyl-4,4'-dicarboxylic acid 4-{[2-[bis-(4-methoxy-phenyl)-phenyl-methoxy]-1-(tert-butyl-dimethyl-silanyloxymethyl)-ethyl]-amide} 4'-({2-[bis-(4-methoxy-phenyl)-phenyl-methoxy]-1-hydroxymethyl-ethyl}-amide)

Base Information

Chemical Name:[2,2']bipyridinyl-4,4'-dicarboxylic acid 4-{[2-[bis-(4-methoxy-phenyl)-phenyl-methoxy]-1-(tert-butyl-dimethyl-silanyloxymethyl)-ethyl]-amide} 4'-({2-[bis-(4-methoxy-phenyl)-phenyl-methoxy]-1-hydroxymethyl-ethyl}-amide)
CAS No.:331465-55-5
Molecular Formula:C₆₆H₇₂N₄O₁₀Si
Molecular Weight:1109.4
Hs Code.:

[2,2']bipyridinyl-4,4'-dicarboxylic acid 4-{[2-[bis-(4-methoxy-phenyl)-phenyl-methoxy]-1-(<i>tert</i>-butyl-dimethyl-silanyloxymethyl)-ethyl]-amide} 4'-({2-[bis-(4-methoxy-phenyl)-phenyl-methoxy]-1-hydroxymethyl-ethyl}-amide)

Synonyms:[2,2']bipyridinyl-4,4'-dicarboxylic acid 4-{[2-[bis-(4-methoxy-phenyl)-phenyl-methoxy]-1-(tert-butyl-dimethyl-silanyloxymethyl)-ethyl]-amide} 4'-({2-[bis-(4-methoxy-phenyl)-phenyl-methoxy]-1-hydroxymethyl-ethyl}-amide)

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Chemical Property of [2,2']bipyridinyl-4,4'-dicarboxylic acid 4-{[2-[bis-(4-methoxy-phenyl)-phenyl-methoxy]-1-(tert-butyl-dimethyl-silanyloxymethyl)-ethyl]-amide} 4'-({2-[bis-(4-methoxy-phenyl)-phenyl-methoxy]-1-hydroxymethyl-ethyl}-amide)

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Technology Process of [2,2']bipyridinyl-4,4'-dicarboxylic acid 4-{[2-[bis-(4-methoxy-phenyl)-phenyl-methoxy]-1-(tert-butyl-dimethyl-silanyloxymethyl)-ethyl]-amide} 4'-({2-[bis-(4-methoxy-phenyl)-phenyl-methoxy]-1-hydroxymethyl-ethyl}-amide)

There total 5 articles about [2,2']bipyridinyl-4,4'-dicarboxylic acid 4-{[2-[bis-(4-methoxy-phenyl)-phenyl-methoxy]-1-(tert-butyl-dimethyl-silanyloxymethyl)-ethyl]-amide} 4'-({2-[bis-(4-methoxy-phenyl)-phenyl-methoxy]-1-hydroxymethyl-ethyl}-amide) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 58.0%

: 18162-48-6
tert-butyldimethylsilyl chloride

: 331465-53-3
[2,2']bipyridinyl-4,4'-dicarboxylic acid bis-({2-[bis-(4-methoxy-phenyl)-phenyl-methoxy]-1-hydroxymethyl-ethyl}-amide)

: 331465-55-5
[2,2']bipyridinyl-4,4'-dicarboxylic acid 4-{[2-[bis-(4-methoxy-phenyl)-phenyl-methoxy]-1-(tert-butyl-dimethyl-silanyloxymethyl)-ethyl]-amide} 4'-({2-[bis-(4-methoxy-phenyl)-phenyl-methoxy]-1-hydroxymethyl-ethyl}-amide)

Guidance literature:: With pyridine; 1H-imidazole; In N,N-dimethyl-formamide; at 20 ℃;
DOI:10.1016/S0960-894X(00)00673-9

Reference yield:

: 40615-36-9
4,4'-dimethoxytrityl chloride

: 331465-55-5
[2,2']bipyridinyl-4,4'-dicarboxylic acid 4-{[2-[bis-(4-methoxy-phenyl)-phenyl-methoxy]-1-(tert-butyl-dimethyl-silanyloxymethyl)-ethyl]-amide} 4'-({2-[bis-(4-methoxy-phenyl)-phenyl-methoxy]-1-hydroxymethyl-ethyl}-amide)

Guidance literature:: Multi-step reaction with 4 steps

1: 59 percent / 4-(dimethylamino)pyridine; pyridine / 2 h

2: 98 percent / piperidine / dimethylformamide / 3 h

3: 85 percent / pyridine / dimethylformamide / 20 °C

4: 58 percent / imidazole; pyridine / dimethylformamide / 20 °C

With piperidine; pyridine; 1H-imidazole; dmap; In N,N-dimethyl-formamide;
DOI:10.1016/S0960-894X(00)00673-9

Reference yield:

: 154928-41-3
2-amino-1-O-(4,4'-dimethoxytrityl)propane-1,3-diol

: 331465-55-5
[2,2']bipyridinyl-4,4'-dicarboxylic acid 4-{[2-[bis-(4-methoxy-phenyl)-phenyl-methoxy]-1-(tert-butyl-dimethyl-silanyloxymethyl)-ethyl]-amide} 4'-({2-[bis-(4-methoxy-phenyl)-phenyl-methoxy]-1-hydroxymethyl-ethyl}-amide)

Guidance literature:: Multi-step reaction with 2 steps

1: 85 percent / pyridine / dimethylformamide / 20 °C

2: 58 percent / imidazole; pyridine / dimethylformamide / 20 °C

With pyridine; 1H-imidazole; In N,N-dimethyl-formamide;
DOI:10.1016/S0960-894X(00)00673-9