N₁,N₆-dimethyl-(2R,3R,4R,5R)-2,5-dibenzyloxy-3,4-dihydroxy hexanediamide

Base Information

Chemical Name:N₁,N₆-dimethyl-(2R,3R,4R,5R)-2,5-dibenzyloxy-3,4-dihydroxy hexanediamide
CAS No.:294867-67-7
Molecular Formula:C₂₂H₂₈N₂O₆
Molecular Weight:416.474
Hs Code.:

N<sub>1</sub>,N<sub>6</sub>-dimethyl-(2R,3R,4R,5R)-2,5-dibenzyloxy-3,4-dihydroxy hexanediamide

Synonyms:N₁,N₆-dimethyl-(2R,3R,4R,5R)-2,5-dibenzyloxy-3,4-dihydroxy hexanediamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N₁,N₆-dimethyl-(2R,3R,4R,5R)-2,5-dibenzyloxy-3,4-dihydroxy hexanediamide

Chemical Property:

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Technology Process of N₁,N₆-dimethyl-(2R,3R,4R,5R)-2,5-dibenzyloxy-3,4-dihydroxy hexanediamide

There total 1 articles about N₁,N₆-dimethyl-(2R,3R,4R,5R)-2,5-dibenzyloxy-3,4-dihydroxy hexanediamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

: 74-89-5
methylamine

: 213895-58-0
2,5-di-O-benzyl-L-mannaro-1,4:3,6-di-γ-lactone

: 294867-67-7
N₁,N₆-dimethyl-(2R,3R,4R,5R)-2,5-dibenzyloxy-3,4-dihydroxy hexanediamide

Guidance literature:: With 2-hydroxypyridin; In tetrahydrofuran; chloroform; at 20 ℃; for 0.25h;
DOI:10.1139/v00-012

Reference yield: 85.0%

: 77-76-9
2,2-dimethoxy-propane

: 294867-67-7
N₁,N₆-dimethyl-(2R,3R,4R,5R)-2,5-dibenzyloxy-3,4-dihydroxy hexanediamide

: 294867-69-9
N₁,N₆-dimethyl-(2R,3R,4R,5R)-2,5-dibenzyloxy-3,4-dihydroxy-3,4-O-isopropylidenehexanediamide

Guidance literature:: With camphor-10-sulfonic acid; In acetone; for 0.25h;
DOI:10.1139/v00-012

Reference yield:

: 294867-67-7
N₁,N₆-dimethyl-(2R,3R,4R,5R)-2,5-dibenzyloxy-3,4-dihydroxy hexanediamide

: N₁-[(1R,2S)-2-hydroxy-2,3-dihydro-1H-indenyl]-N₆-(isobutyl)-(2R,3R,4R,5R)-2,5-dibenzyloxy-3,4-O-isopropylidenehexanediamide

Guidance literature:: Multi-step reaction with 4 steps

1: 85 percent / camphorsulfonic acid / acetone / 0.25 h

2: N₂O₄; Pb(NO₃)2; NaOAc / CH₂Cl₂ / 1.5 h / -60 - -10 °C

3: 100 percent / 30 percent aq. H₂O₂; LiOH / tetrahydrofuran / 0.33 h / 0 °C

With lithium hydroxide; lead(II) nitrate; camphor-10-sulfonic acid; dihydrogen peroxide; sodium acetate; dinitrogen tetraoxide; In tetrahydrofuran; dichloromethane; acetone; 1: Condensation / 2: Nitrosation / 3: Oxidation;
DOI:10.1139/v00-012