Methyl-(4-aminomethyl)cyclohexane carboxylate hydrochloride salt 95%

Base Information

• Chemical Name: Methyl-(4-aminomethyl)cyclohexane carboxylate hydrochloride salt 95%
• CAS No.: 54640-02-7
• Molecular Formula: C9H17NO2.ClH
• Molecular Weight: 207.7
• Hs Code.: 2922499990
• Mol file: 54640-02-7.mol

Synonyms:Methyl-(4-aminomethyl)cyclohexane carboxylate hydrochloride salt 95%

Chemical Property of Methyl-(4-aminomethyl)cyclohexane carboxylate hydrochloride salt 95%

Chemical Property:

• PSA: 52.32000
• LogP: 2.42680
• Storage Temp.: Inert atmosphere,Room Temperature
• Water Solubility.: Soluble in water

Purity/Quality:

97% ^*data from raw suppliers

Methyl 4-(Aminomethyl)cyclohexanecarboxylate Hydrochloride (cis- and trans- mixture) >98.0%(T) ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of Methyl-(4-aminomethyl)cyclohexane carboxylate hydrochloride salt 95%

There total 4 articles about Methyl-(4-aminomethyl)cyclohexane carboxylate hydrochloride salt 95% which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

methanol (67-56-1) + 4-aminomethyl-cyclohexanecarboxylic acid (1197-17-7,1197-18-8,701-54-2) → 4-aminomethylcyclohexanecarboxylic acid methyl ester hydrochloride salt (54640-02-7,29275-88-5)

Guidance literature:

With thionyl chloride; at -10 - 20 ℃; for 20h;

Reference yield: 98.0%

tert-butyl methyl ether (1634-04-4) + 4-aminomethyl-cyclohexanecarboxylic acid (1197-17-7,1197-18-8,701-54-2) → 4-aminomethylcyclohexanecarboxylic acid methyl ester hydrochloride salt (54640-02-7,29275-88-5)

Guidance literature:

4-aminomethyl-cyclohexanecarboxylic acid; In methanol; at 5 ℃; for 0.166667h; Inert atmosphere; Large scale;

With thionyl chloride; In methanol; at 10 - 25 ℃; for 3.5h; Inert atmosphere; Large scale;

tert-butyl methyl ether; at -5 - 30 ℃; for 1.45h; Temperature; Time; Reagent/catalyst; Large scale;

DOI:10.1021/op400145w

Reference yield:

4-aminomethyl-cyclohexanecarboxylic acid (1197-17-7,1197-18-8,701-54-2) + 2,2-dimethoxy-propane (77-76-9) → 4-aminomethylcyclohexanecarboxylic acid methyl ester hydrochloride salt (54640-02-7,29275-88-5)

Guidance literature:

With hydrogenchloride; In water; at 20 ℃; for 18h;

upstream raw materials:

methanol

4-aminomethyl-cyclohexanecarboxylic acid

tert-butyl methyl ether

2,2-dimethoxy-propane

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