N-(4-(9H-carbazol-9-yl)phenyl)-4-nitro-N-(4-nitrophenyl)aniline

Base Information

• Chemical Name: N-(4-(9H-carbazol-9-yl)phenyl)-4-nitro-N-(4-nitrophenyl)aniline
• CAS No.: 896452-73-6
• Molecular Formula: C₃₀H₂₀N₄O₄
• Molecular Weight: 500.513
• Mol file: 896452-73-6.mol

Synonyms:N-(4-(9H-carbazol-9-yl)phenyl)-4-nitro-N-(4-nitrophenyl)aniline

Chemical Property of N-(4-(9H-carbazol-9-yl)phenyl)-4-nitro-N-(4-nitrophenyl)aniline

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of N-(4-(9H-carbazol-9-yl)phenyl)-4-nitro-N-(4-nitrophenyl)aniline

There total 5 articles about N-(4-(9H-carbazol-9-yl)phenyl)-4-nitro-N-(4-nitrophenyl)aniline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.4%

4-(9H-carbazol-9-yl)aniline (52708-37-9) + 4-Fluoronitrobenzene (350-46-9,178603-76-4) → N-(4-(9H-carbazol-9-yl)phenyl)-4-nitro-N-(4-nitrophenyl)aniline (896452-73-6)

Guidance literature:

With potassium carbonate; In N,N-dimethyl-formamide; at 100 ℃; for 12h; Inert atmosphere;

DOI:10.1080/15421406.2020.1743429

Reference yield:

9-(4-nitrophenyl)-9H-carbazole (16982-76-6) → N-(4-(9H-carbazol-9-yl)phenyl)-4-nitro-N-(4-nitrophenyl)aniline (896452-73-6)

Guidance literature:

Multi-step reaction with 2 steps

1: hydrazine monohydrate / Pd/C / ethanol / 9 h / Heating

2: 78 percent / caesium fluoride / dimethylsulfoxide / 15 h / 150 °C

With hydrazine hydrate; cesium fluoride; palladium on activated charcoal; In ethanol; dimethyl sulfoxide;

DOI:10.1039/b602133f

Reference yield:

4-Fluoronitrobenzene (350-46-9,178603-76-4) → N-(4-(9H-carbazol-9-yl)phenyl)-4-nitro-N-(4-nitrophenyl)aniline (896452-73-6)

Guidance literature:

Multi-step reaction with 3 steps

1: 98 percent / caesium fluoride / dimethylsulfoxide / 15 h / 150 °C

2: hydrazine monohydrate / Pd/C / ethanol / 9 h / Heating

3: 78 percent / caesium fluoride / dimethylsulfoxide / 15 h / 150 °C

With hydrazine hydrate; cesium fluoride; palladium on activated charcoal; In ethanol; dimethyl sulfoxide;

DOI:10.1039/b602133f

upstream raw materials:

4-(9H-carbazol-9-yl)aniline

4-Fluoronitrobenzene

9-(4-nitrophenyl)-9H-carbazole

9H-carbazole

Downstream raw materials:

N¹-(4-(9H-carbazol-9-yl)phenyl)-N₁-(4-aminophenyl)benzene-1,4-diamine