4-(9H-Carbazol-9-yl)aniline

Base Information

• Chemical Name: 4-(9H-Carbazol-9-yl)aniline
• CAS No.: 52708-37-9
• Molecular Formula: C18H14N2
• Molecular Weight: 258.323
• Hs Code.: 2933990090
• European Community (EC) Number: 835-533-5
• DSSTox Substance ID: DTXSID70347398
• Nikkaji Number: J1.255.004I
• Wikidata: Q82121269
• Mol file: 52708-37-9.mol

Synonyms:4-(9H-Carbazol-9-yl)aniline;52708-37-9;4-carbazol-9-ylaniline;4-(Carbazol-9-yl)aniline;n-(4-aminophenyl)carbazole;Benzenamine, 4-(9H-carbazol-9-yl)-;4-(9H-carbazol-9-yl)benzenamine;Oprea1_417247;Oprea1_639139;SCHEMBL997011;4-(9H-Carbazole-9-yl)aniline;DTXSID70347398;4-(9H-Carbazol-9-yl)aniline #;CCA70837;MFCD00626047;AKOS000733281;AS-59140;C3082;CS-0378202;EU-0050678;T71004;A923386;SR-01000508324;SR-01000508324-1

Chemical Property of 4-(9H-Carbazol-9-yl)aniline

Chemical Property:

• Melting Point: 96 °C
• Boiling Point: 475.0±37.0 °C(Predicted)
• PKA: 3.47±0.10(Predicted)
• PSA: 30.95000
• Density: 1.19±0.1 g/cm3(Predicted)
• LogP: 4.94710
• Storage Temp.: 2-8°C
• Solubility.: soluble in Toluene
• XLogP3: 4.3
• Hydrogen Bond Donor Count: 1
• Hydrogen Bond Acceptor Count: 1
• Rotatable Bond Count: 1
• Exact Mass: 258.115698455
• Heavy Atom Count: 20
• Complexity: 312

Purity/Quality:

97% ^*data from raw suppliers

4-(Carbazol-9-yl)aniline ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

• Canonical SMILES: C1=CC=C2C(=C1)C3=CC=CC=C3N2C4=CC=C(C=C4)N
• Uses: 4-(Carbazol-9-yl)aniline

Technology Process of 4-(9H-Carbazol-9-yl)aniline

There total 25 articles about 4-(9H-Carbazol-9-yl)aniline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

9-(4-nitrophenyl)-9H-carbazole (16982-76-6) → 4-(9H-carbazol-9-yl)aniline (52708-37-9)

Guidance literature:

With palladium on activated charcoal; hydrazine hydrate; In ethanol; Reflux; Inert atmosphere;

DOI:10.1039/c7ra09558a

Reference yield: 99.0%

9-((4-acetamido)phenyl)carbazole (57103-11-4) → 4-(9H-carbazol-9-yl)aniline (52708-37-9)

Guidance literature:

With sulfuric acid; In tetrahydrofuran; methanol; water; for 2h; Heating;

DOI:10.1021/ma0499674

Reference yield: 92.0%

9H-carbazole (86-74-8,105184-46-1,97960-57-1) + p-aminoiodobenzene (540-37-4) → 4-(9H-carbazol-9-yl)aniline (52708-37-9)

Guidance literature:

With copper(I) oxide; In diphenylether; at 190 ℃; for 24h;

upstream raw materials:

9-(4-nitrophenyl)-9H-carbazole

9-((4-acetamido)phenyl)carbazole

p-nitrobenzene iodide

9H-carbazole

Downstream raw materials:

(4-carbazol-9-yl-phenyl)-(2-nitro-phenyl)-amine

N-(4-(9H-carbazol-9-yl)phenyl)-4-nitro-N-(4-nitrophenyl)aniline

9-(4-iodophenyl)carbazole

N¹-(4-(9H-carbazol-9-yl)phenyl)-N₁-(4-aminophenyl)benzene-1,4-diamine