3'-(chloromethyl)-2,6-dimethyl-4-(3-(methylsulfonyl)propoxy)-1,1'-biphenyl

Base Information

Chemical Name:3'-(chloromethyl)-2,6-dimethyl-4-(3-(methylsulfonyl)propoxy)-1,1'-biphenyl
CAS No.:1394138-49-8
Molecular Formula:C₁₉H₂₃ClO₃S
Molecular Weight:366.909
Hs Code.:2909309090

Synonyms:3'-(chloromethyl)-2,6-dimethyl-4-(3-(methylsulfonyl)propoxy)-1,1'-biphenyl

Suppliers and Price of 3'-(chloromethyl)-2,6-dimethyl-4-(3-(methylsulfonyl)propoxy)-1,1'-biphenyl

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Crysdot
3'-(CHLOROMETHYL)-2,6-DIMETHYL-4-(3-(METHYLSULFONYL)PROPOXY)-1,1'-BIPHENYL 95+%
1g
$ 559.00

Apolloscientific
3'-(Chloromethyl)-2,6-dimethyl-4-[3-(methylsulfonyl)propoxy]biphenyl
5g
$ 3248.00

Apolloscientific
3'-(Chloromethyl)-2,6-dimethyl-4-[3-(methylsulfonyl)propoxy]biphenyl
1g
$ 1208.00

Apolloscientific
3'-(Chloromethyl)-2,6-dimethyl-4-[3-(methylsulfonyl)propoxy]biphenyl
250mg
$ 518.00

Total 6 raw suppliers

Chemical Property of 3'-(chloromethyl)-2,6-dimethyl-4-(3-(methylsulfonyl)propoxy)-1,1'-biphenyl

Chemical Property:

Purity/Quality:

97% ^*data from raw suppliers

3'-(CHLOROMETHYL)-2,6-DIMETHYL-4-(3-(METHYLSULFONYL)PROPOXY)-1,1'-BIPHENYL 95+% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 3'-(chloromethyl)-2,6-dimethyl-4-(3-(methylsulfonyl)propoxy)-1,1'-biphenyl

There total 5 articles about 3'-(chloromethyl)-2,6-dimethyl-4-(3-(methylsulfonyl)propoxy)-1,1'-biphenyl which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1000413-85-3
(2’,6’-dimethyl-4’-(3-(methylsulfonyl)propoxy)-[1,1‘-biphenyl]-3-yl)methanol

: 1394138-49-8
3'-(chloromethyl)-2,6-dimethyl-4-(3-(methylsulfonyl)propoxy)-1,1'-biphenyl

Guidance literature:: With trichlorophosphate; N,N-dimethyl-formamide; at 25 ℃; for 1h;

Reference yield:

: 1000413-84-2
2',6'-dimethyl-4'-(3-(methylsulfonyl)propoxy)-[1,1'-biphenyl]-3-carbaldehyde

: 1394138-49-8
3'-(chloromethyl)-2,6-dimethyl-4-(3-(methylsulfonyl)propoxy)-1,1'-biphenyl

Guidance literature:: Multi-step reaction with 2 steps

1: sodium hydroxide; water; sodium tetrahydroborate / ethanol / 1 h / 25 °C

2: trichlorophosphate / N,N-dimethyl-formamide / 1 h / 25 °C

With sodium tetrahydroborate; water; sodium hydroxide; trichlorophosphate; N,N-dimethyl-formamide; In ethanol;

Reference yield:

: 1372195-69-1
2-bromo-5-(3-methanesulfonyl-propoxy)-1,3-dimethyl-benzene

: 1394138-49-8
3'-(chloromethyl)-2,6-dimethyl-4-(3-(methylsulfonyl)propoxy)-1,1'-biphenyl

Guidance literature:: Multi-step reaction with 2 steps

1: potassium phosphate / triphenylphosphine; palladium diacetate; tetrabutylammomium bromide / tetrahydrofuran / 8 h / Reflux; Inert atmosphere

2: trichlorophosphate / N,N-dimethyl-formamide / 1 h / 25 °C

With potassium phosphate; trichlorophosphate; tetrabutylammomium bromide; palladium diacetate; N,N-dimethyl-formamide; triphenylphosphine; In tetrahydrofuran;