4-((E)-3-(4-(4-(2-hydroxyethyl)piperidin-1-yl)butoxy)-3-oxoprop-1-enyl)-2-methoxyphenyl2-((2E,6E)-3,7,11-trimethyldodeca-2,6,10-trienylthio)benzoate

Base Information

Chemical Name:4-((E)-3-(4-(4-(2-hydroxyethyl)piperidin-1-yl)butoxy)-3-oxoprop-1-enyl)-2-methoxyphenyl2-((2E,6E)-3,7,11-trimethyldodeca-2,6,10-trienylthio)benzoate
CAS No.:1613704-92-9
Molecular Formula:C₄₂H₅₈N₂O₆S
Molecular Weight:718.998
Hs Code.:

Synonyms:4-((E)-3-(4-(4-(2-hydroxyethyl)piperidin-1-yl)butoxy)-3-oxoprop-1-enyl)-2-methoxyphenyl2-((2E,6E)-3,7,11-trimethyldodeca-2,6,10-trienylthio)benzoate

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Chemical Property of 4-((E)-3-(4-(4-(2-hydroxyethyl)piperidin-1-yl)butoxy)-3-oxoprop-1-enyl)-2-methoxyphenyl2-((2E,6E)-3,7,11-trimethyldodeca-2,6,10-trienylthio)benzoate

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Technology Process of 4-((E)-3-(4-(4-(2-hydroxyethyl)piperidin-1-yl)butoxy)-3-oxoprop-1-enyl)-2-methoxyphenyl2-((2E,6E)-3,7,11-trimethyldodeca-2,6,10-trienylthio)benzoate

There total 2 articles about 4-((E)-3-(4-(4-(2-hydroxyethyl)piperidin-1-yl)butoxy)-3-oxoprop-1-enyl)-2-methoxyphenyl2-((2E,6E)-3,7,11-trimethyldodeca-2,6,10-trienylthio)benzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 52.0%

: 103-76-4
1-(2-hydroxyethyl)piperazine

: 1613704-90-7
4-((E)-3-(4-bromobutoxy)-3-oxoprop-1-enyl)-2-methoxyphenyl-2-((2E,6E)-3,7,11-trimethyldodeca-2,6,10-trienylthio)benzoate

: 1613704-92-9
4-((E)-3-(4-(4-(2-hydroxyethyl)piperidin-1-yl)butoxy)-3-oxoprop-1-enyl)-2-methoxyphenyl2-((2E,6E)-3,7,11-trimethyldodeca-2,6,10-trienylthio)benzoate

Guidance literature:: With potassium carbonate; potassium iodide; In acetonitrile; at 50 ℃; for 6h;
DOI:10.1039/c4ob00023d

Reference yield:

: 1135-24-6,537-98-4
(E)-3-(4-hydroxy-3-methoxyphenyl)acrylic acid

: 1613704-92-9
4-((E)-3-(4-(4-(2-hydroxyethyl)piperidin-1-yl)butoxy)-3-oxoprop-1-enyl)-2-methoxyphenyl2-((2E,6E)-3,7,11-trimethyldodeca-2,6,10-trienylthio)benzoate

Guidance literature:: Multi-step reaction with 3 steps

1: triethylamine / acetone / 4 h / 50 °C

2: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; dmap / dichloromethane / 28 h / 20 °C

3: potassium iodide; potassium carbonate / acetonitrile / 6 h / 50 °C

With dmap; potassium carbonate; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; potassium iodide; In dichloromethane; acetone; acetonitrile;
DOI:10.1039/c4ob00023d