2-(4-morpholinyl)-2-<2-phenyl-1-(phenylmethyl)-1H-imidazol-4-yl>pentanedinitrile

Base Information

Chemical Name:2-(4-morpholinyl)-2-<2-phenyl-1-(phenylmethyl)-1H-imidazol-4-yl>pentanedinitrile
CAS No.:99280-91-8
Molecular Formula:C₂₅H₂₅N₅O
Molecular Weight:411.506
Hs Code.:

Synonyms:2-(4-morpholinyl)-2-<2-phenyl-1-(phenylmethyl)-1H-imidazol-4-yl>pentanedinitrile

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2-(4-morpholinyl)-2-<2-phenyl-1-(phenylmethyl)-1H-imidazol-4-yl>pentanedinitrile

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Technology Process of 2-(4-morpholinyl)-2-<2-phenyl-1-(phenylmethyl)-1H-imidazol-4-yl>pentanedinitrile

There total 5 articles about 2-(4-morpholinyl)-2-<2-phenyl-1-(phenylmethyl)-1H-imidazol-4-yl>pentanedinitrile which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 99280-87-2
α-<2-phenyl-1-(phenylmethyl)-1H-imidazol-4-yl>-4-morpholineacetonitrile

: 107-13-1,25014-41-9
acrylonitrile

: 99280-91-8
2-(4-morpholinyl)-2-<2-phenyl-1-(phenylmethyl)-1H-imidazol-4-yl>pentanedinitrile

Guidance literature:: With potassium hydroxide; In tetrahydrofuran; methanol; at 23 ℃; for 2h;
DOI:10.1021/jm00152a015

Reference yield:

: 100-39-0
benzyl bromide

: 99280-91-8
2-(4-morpholinyl)-2-<2-phenyl-1-(phenylmethyl)-1H-imidazol-4-yl>pentanedinitrile

Guidance literature:: Multi-step reaction with 4 steps

1: 60 percent / KOH / dimethylformamide / 5 h / 55 °C

2: MnO₂ / tetrahydrofuran / 1.5 h / Heating

3: p-toluenesulfonic acid monohydrate / dioxane / 1.5 h / Heating

4: KOH / tetrahydrofuran; methanol / 2 h / 23 °C

With manganese(IV) oxide; potassium hydroxide; toluene-4-sulfonic acid; In tetrahydrofuran; 1,4-dioxane; methanol; N,N-dimethyl-formamide;
DOI:10.1021/jm00152a015

Reference yield:

: 99280-85-0
1-benzyl-2-phenyl-1H-imidazole-4-carbaldehyde

: 99280-91-8
2-(4-morpholinyl)-2-<2-phenyl-1-(phenylmethyl)-1H-imidazol-4-yl>pentanedinitrile

Guidance literature:: Multi-step reaction with 2 steps

1: p-toluenesulfonic acid monohydrate / dioxane / 1.5 h / Heating

2: KOH / tetrahydrofuran; methanol / 2 h / 23 °C

With potassium hydroxide; toluene-4-sulfonic acid; In tetrahydrofuran; 1,4-dioxane; methanol;
DOI:10.1021/jm00152a015