4-((R)-1-methanesulfonyloxy-ethyl)piperidine-1-carboxylic acid benzyl ester

Base Information

Chemical Name:4-((R)-1-methanesulfonyloxy-ethyl)piperidine-1-carboxylic acid benzyl ester
CAS No.:1351343-15-1
Molecular Formula:C₁₆H₂₃NO₅S
Molecular Weight:341.428
Hs Code.:

Synonyms:4-((R)-1-methanesulfonyloxy-ethyl)piperidine-1-carboxylic acid benzyl ester

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Chemical Property of 4-((R)-1-methanesulfonyloxy-ethyl)piperidine-1-carboxylic acid benzyl ester

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Technology Process of 4-((R)-1-methanesulfonyloxy-ethyl)piperidine-1-carboxylic acid benzyl ester

There total 3 articles about 4-((R)-1-methanesulfonyloxy-ethyl)piperidine-1-carboxylic acid benzyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 27854-88-2,42732-22-9
(R)-1-(4-pyridinyl)ethanol

: 1351343-15-1
4-((R)-1-methanesulfonyloxy-ethyl)piperidine-1-carboxylic acid benzyl ester

Guidance literature:: Multi-step reaction with 3 steps

1.1: hydrogen / platinum oxide / methanol / 18 h / 38002.6 Torr / Inert atmosphere

2.1: sodium carbonate / dichloromethane; water / 16 h / 20 °C

3.1: triethylamine / dichloromethane / 0.5 h / 0 °C

3.2: 4 h / 0 - 20 °C

With hydrogen; sodium carbonate; triethylamine; platinum oxide; In methanol; dichloromethane; water;

Reference yield:

: 1122-54-9
methyl (4-pyridyl) ketone

: 1351343-15-1
4-((R)-1-methanesulfonyloxy-ethyl)piperidine-1-carboxylic acid benzyl ester

Guidance literature:: Multi-step reaction with 4 steps

1.1: dimethylsulfide borane complex; Trimethyl borate; (S)-diphenylprolinol / tetrahydrofuran / 0 - 20 °C

2.1: hydrogen / platinum oxide / methanol / 18 h / 38002.6 Torr / Inert atmosphere

3.1: sodium carbonate / dichloromethane; water / 16 h / 20 °C

4.1: triethylamine / dichloromethane / 0.5 h / 0 °C

4.2: 4 h / 0 - 20 °C

With Trimethyl borate; (S)-diphenylprolinol; dimethylsulfide borane complex; hydrogen; sodium carbonate; triethylamine; platinum oxide; In tetrahydrofuran; methanol; dichloromethane; water;

Reference yield:

: 1032825-62-9
(1R)-1-(4-piperidinyl)ethanol acetic acid salt

: 1351343-15-1
4-((R)-1-methanesulfonyloxy-ethyl)piperidine-1-carboxylic acid benzyl ester

Guidance literature:: Multi-step reaction with 2 steps

1.1: sodium carbonate / dichloromethane; water / 16 h / 20 °C

2.1: triethylamine / dichloromethane / 0.5 h / 0 °C

2.2: 4 h / 0 - 20 °C

With sodium carbonate; triethylamine; In dichloromethane; water;