1,4-bis(diphenylfluorostannyl)butane

Base Information

Chemical Name:1,4-bis(diphenylfluorostannyl)butane
CAS No.:223668-35-7
Molecular Formula:C₂₈H₂₈F₂Sn₂
Molecular Weight:639.947
Hs Code.:

Synonyms:1,4-bis(diphenylfluorostannyl)butane

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1,4-bis(diphenylfluorostannyl)butane

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Technology Process of 1,4-bis(diphenylfluorostannyl)butane

There total 1 articles about 1,4-bis(diphenylfluorostannyl)butane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 7789-23-3
potassium fluoride

: 5274-40-8
1,4-bis(triphenylstannyl)butane

: 223668-35-7
1,4-bis(diphenylfluorostannyl)butane

Guidance literature:: With I₂; In dichloromethane; water; byproducts: iodobenzene; dropwise addn. of 2 equiv. of I2 to Sn-compd. at 0°C, stirring (room temp., 16 h), solvent removal, distn. off of C6H5I (60°C, 1E-3 Torr), dissoln. in Me2CO, dropwise addn. of excess of aq. KF, stirring(room temp., 4 h); filtration, washing (H2O, Et2O);
DOI:10.1016/S0022-328X(98)00935-8

Reference yield: 83.0%

: 630-17-1
2,2-dimethylpropyl bromide

: 223668-35-7
1,4-bis(diphenylfluorostannyl)butane

: 223668-38-0
((C₆H₅)2(CH₂C(CH₃)3)SnCH₂CH₂)2

Guidance literature:: With Mg; In tetrahydrofuran; dropwise addn. of Sn-compd. to 2 equiv. of Grignard reagent (prepd. fromMg and Me3CCH2Br), refluxing for 1 d; addn. of satd. NH4Cl soln., extn. into Et2O, drying (Na2SO4), filtration, solvent removal (vac.); elem. anal.;
DOI:10.1016/S0022-328X(98)00935-8