C₃₀H₃₃N₅O₃

Base Information

Chemical Name:C₃₀H₃₃N₅O₃
CAS No.:1312938-96-7
Molecular Formula:C₃₀H₃₃N₅O₃
Molecular Weight:511.624
Hs Code.:

C<sub>30</sub>H<sub>33</sub>N<sub>5</sub>O<sub>3</sub>

Synonyms:C₃₀H₃₃N₅O₃

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Chemical Property of C₃₀H₃₃N₅O₃

Chemical Property:

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Technology Process of C₃₀H₃₃N₅O₃

There total 6 articles about C₃₀H₃₃N₅O₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1312938-95-6
4'-{[4-butyl-1-(5-ethoxypyrimidin-2-yl)-6-methyl-2-oxo-1,2-dihydropyridin-3-yl]methyl}biphenyl-2-carbonitrile

: 1312938-96-7
C₃₀H₃₃N₅O₃

Guidance literature:: With hydroxylamine hydrochloride; sodium hydrogencarbonate; In dimethyl sulfoxide; at 40 ℃; for 1h;

4'-{[4-butyl-1-(5-ethoxypyrimidin-2-yl)-6-methyl-2-oxo-1,2-dihydropyridin-3-yl]methyl}biphenyl-2-carbonitrile; In dimethyl sulfoxide; at 90 ℃; for 16h;

Reference yield:

: 1312938-92-3
3-acetyl-1-(5-ethoxypyrimidin-2-yl)-4-hydroxy-6-methylpyridin-2(1H)-one

: 1312938-96-7
C₃₀H₃₃N₅O₃

Guidance literature:: Multi-step reaction with 5 steps

1.1: sulfuric acid / water / 0.25 h / 150 °C

1.2: pH 8 / Cooling with ice

2.1: lithium chloride / N,N-dimethyl-formamide / 70 °C

3.1: pyridine / dichloromethane / 2 h / 20 °C

4.1: palladium bis[bis(diphenylphosphino)ferrocene] dichloride / toluene; tetrahydrofuran / 1.5 h / 0 - 90 °C / Inert atmosphere

5.1: hydroxylamine hydrochloride; sodium hydrogencarbonate / dimethyl sulfoxide / 1 h / 40 °C

5.2: 16 h / 90 °C

With pyridine; sulfuric acid; hydroxylamine hydrochloride; sodium hydrogencarbonate; lithium chloride; palladium bis[bis(diphenylphosphino)ferrocene] dichloride; In tetrahydrofuran; dichloromethane; water; dimethyl sulfoxide; N,N-dimethyl-formamide; toluene;

Reference yield:

: 1312938-93-4
1-(5-ethoxypyrimidin-2-yl)-4-hydroxy-6-methylpyridin-2(1H)-one

: 1312938-96-7
C₃₀H₃₃N₅O₃

Guidance literature:: Multi-step reaction with 4 steps

1.1: lithium chloride / N,N-dimethyl-formamide / 70 °C

2.1: pyridine / dichloromethane / 2 h / 20 °C

3.1: palladium bis[bis(diphenylphosphino)ferrocene] dichloride / toluene; tetrahydrofuran / 1.5 h / 0 - 90 °C / Inert atmosphere

4.1: hydroxylamine hydrochloride; sodium hydrogencarbonate / dimethyl sulfoxide / 1 h / 40 °C

4.2: 16 h / 90 °C

With pyridine; hydroxylamine hydrochloride; sodium hydrogencarbonate; lithium chloride; palladium bis[bis(diphenylphosphino)ferrocene] dichloride; In tetrahydrofuran; dichloromethane; dimethyl sulfoxide; N,N-dimethyl-formamide; toluene;