N′-methyl-N′-{2-chloro-5-[5-(3,5-dichlorophenyl)-5-trifluoro methyl-4,5-dihydroisoxazol-3-yl]phenyl}cyclopropanecarbohydrazide

Base Information

Chemical Name:N′-methyl-N′-{2-chloro-5-[5-(3,5-dichlorophenyl)-5-trifluoro methyl-4,5-dihydroisoxazol-3-yl]phenyl}cyclopropanecarbohydrazide
CAS No.:1237587-40-4
Molecular Formula:C₂₁H₁₇Cl₃F₃N₃O₂
Molecular Weight:506.739
Hs Code.:

Synonyms:N′-methyl-N′-{2-chloro-5-[5-(3,5-dichlorophenyl)-5-trifluoro methyl-4,5-dihydroisoxazol-3-yl]phenyl}cyclopropanecarbohydrazide

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Chemical Property of N′-methyl-N′-{2-chloro-5-[5-(3,5-dichlorophenyl)-5-trifluoro methyl-4,5-dihydroisoxazol-3-yl]phenyl}cyclopropanecarbohydrazide

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Technology Process of N′-methyl-N′-{2-chloro-5-[5-(3,5-dichlorophenyl)-5-trifluoro methyl-4,5-dihydroisoxazol-3-yl]phenyl}cyclopropanecarbohydrazide

There total 11 articles about N′-methyl-N′-{2-chloro-5-[5-(3,5-dichlorophenyl)-5-trifluoro methyl-4,5-dihydroisoxazol-3-yl]phenyl}cyclopropanecarbohydrazide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1237587-92-6
N-methyl-N-{2-chloro-5-[5-(3,5-dichlorophenyl)-5-trifluoromethyl-4,5-dihydroisoxazol-3-yl]phenyl}hydrazine

: 4023-34-1
cyclopropanecarboxylic acid chloride

: 1237587-40-4
N′-methyl-N′-{2-chloro-5-[5-(3,5-dichlorophenyl)-5-trifluoro methyl-4,5-dihydroisoxazol-3-yl]phenyl}cyclopropanecarbohydrazide

Guidance literature:: With triethylamine; In tetrahydrofuran; at 20 ℃;

Reference yield:

: 1071928-04-5
5-[5-(3,5-dichlorophenyl)-5-trifluoromethyl-4,5-dihydroisoxazol-3-yl]-2-chloronitrobenzene

: 1237587-40-4
N′-methyl-N′-{2-chloro-5-[5-(3,5-dichlorophenyl)-5-trifluoro methyl-4,5-dihydroisoxazol-3-yl]phenyl}cyclopropanecarbohydrazide

Guidance literature:: Multi-step reaction with 7 steps

1.1: acetic acid; iron / ethanol; water / 0.83 h / 75 °C

2.1: triethylamine / tetrahydrofuran / 0.5 h / 0 °C

3.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 0.33 h / 20 °C

3.2: 1 h

4.1: potassium carbonate; methanol / 3 h / 20 °C

5.1: hydrogenchloride / water; tetrahydrofuran / 0.17 h / 20 °C

5.2: 1 h / 0 °C

6.1: zinc; acetic acid / ethanol; water; tetrahydrofuran / 3 h / 20 °C

7.1: triethylamine / tetrahydrofuran / 0.5 h / 20 °C

With hydrogenchloride; methanol; iron; sodium hydride; potassium carbonate; acetic acid; triethylamine; zinc; In tetrahydrofuran; ethanol; water; N,N-dimethyl-formamide; mineral oil;

Reference yield:

: 864725-22-4
1,3-dichloro-5-(3,3,3-trifluoroprop-1-en-2-yl)benzene

: 1237587-40-4
N′-methyl-N′-{2-chloro-5-[5-(3,5-dichlorophenyl)-5-trifluoro methyl-4,5-dihydroisoxazol-3-yl]phenyl}cyclopropanecarbohydrazide

Guidance literature:: Multi-step reaction with 8 steps

1.1: N-chloro-succinimide / N,N-dimethyl-formamide / 1 h / 60 °C

1.2: 6 h / 20 °C

2.1: acetic acid; iron / ethanol; water / 0.83 h / 75 °C

3.1: triethylamine / tetrahydrofuran / 0.5 h / 0 °C

4.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 0.33 h / 20 °C

4.2: 1 h

5.1: potassium carbonate; methanol / 3 h / 20 °C

6.1: hydrogenchloride / water; tetrahydrofuran / 0.17 h / 20 °C

6.2: 1 h / 0 °C

7.1: zinc; acetic acid / ethanol; water; tetrahydrofuran / 3 h / 20 °C

8.1: triethylamine / tetrahydrofuran / 0.5 h / 20 °C

With hydrogenchloride; methanol; N-chloro-succinimide; iron; sodium hydride; potassium carbonate; acetic acid; triethylamine; zinc; In tetrahydrofuran; ethanol; water; N,N-dimethyl-formamide; mineral oil;