cis-2-bromomethyl-2-(2,4-dichlorophenyl)-4-phenylcarbonyloxymethyl-1,3-dioxolane

Base Information

Chemical Name:cis-2-bromomethyl-2-(2,4-dichlorophenyl)-4-phenylcarbonyloxymethyl-1,3-dioxolane
CAS No.:170210-46-5
Molecular Formula:C₁₈H₁₅BrCl₂O₄
Molecular Weight:446.125
Hs Code.:

Synonyms:cis-2-bromomethyl-2-(2,4-dichlorophenyl)-4-phenylcarbonyloxymethyl-1,3-dioxolane

Suppliers and Price of cis-2-bromomethyl-2-(2,4-dichlorophenyl)-4-phenylcarbonyloxymethyl-1,3-dioxolane

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Total 2 raw suppliers

Chemical Property of cis-2-bromomethyl-2-(2,4-dichlorophenyl)-4-phenylcarbonyloxymethyl-1,3-dioxolane

Chemical Property:

Purity/Quality:: 98% ^*data from raw suppliers

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Technology Process of cis-2-bromomethyl-2-(2,4-dichlorophenyl)-4-phenylcarbonyloxymethyl-1,3-dioxolane

There total 6 articles about cis-2-bromomethyl-2-(2,4-dichlorophenyl)-4-phenylcarbonyloxymethyl-1,3-dioxolane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₁₈H₁₅BrCl₂O₄

: 170210-46-5
cis-2-bromomethyl-2-(2,4-dichlorophenyl)-4-phenylcarbonyloxymethyl-1,3-dioxolane

Guidance literature:: C₁₈H₁₅BrCl₂O₄; In methanol; at 25 ℃; for 1h;

With tert-butyl methyl ether; In methanol; at 60 ℃; for 0.5h;

Reference yield:

: 2631-72-3
2,4-dichlorophenacyl bromide

: 170210-46-5
cis-2-bromomethyl-2-(2,4-dichlorophenyl)-4-phenylcarbonyloxymethyl-1,3-dioxolane

Guidance literature:: Multi-step reaction with 2 steps

1: p-TsOH*H₂O / toluene; butan-1-ol / 24 h / Heating

2: dimethylformamide / 6 h / 160 - 165 °C

With toluene-4-sulfonic acid; In N,N-dimethyl-formamide; toluene; butan-1-ol;
DOI:10.1016/0957-4166(95)00161-H

Reference yield:

: 2234-16-4
1-(2,4-dichlorophenyl)ethan-1-one

: 170210-46-5
cis-2-bromomethyl-2-(2,4-dichlorophenyl)-4-phenylcarbonyloxymethyl-1,3-dioxolane

Guidance literature:: Multi-step reaction with 4 steps

1.1: N-Bromosuccinimide / acetonitrile / 1 h / 20 - 25 °C

1.2: 5 h / 90 °C

2.1: toluene-4-sulfonic acid / toluene; butan-1-ol / 36 h / 130 °C

3.1: N,N-dimethyl-formamide / 5 h / 160 - 165 °C

4.1: methanol / 1 h / 25 °C

4.2: 0.5 h / 60 °C

With N-Bromosuccinimide; toluene-4-sulfonic acid; In methanol; N,N-dimethyl-formamide; toluene; acetonitrile; butan-1-ol;