3,4,6-tri-O-acetyl-2-deoxy-2-(4-methoxybenzyl)imino-α-D-glucopyranosyl bromide

Base Information

• Chemical Name: 3,4,6-tri-O-acetyl-2-deoxy-2-(4-methoxybenzyl)imino-α-D-glucopyranosyl bromide
• CAS No.: 61567-93-9
• Molecular Formula: C₂₀H₂₄BrNO₈
• Molecular Weight: 486.316

Synonyms:3,4,6-tri-O-acetyl-2-deoxy-2-(4-methoxybenzyl)imino-α-D-glucopyranosyl bromide

Chemical Property of 3,4,6-tri-O-acetyl-2-deoxy-2-(4-methoxybenzyl)imino-α-D-glucopyranosyl bromide

Chemical Property:

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Technology Process of 3,4,6-tri-O-acetyl-2-deoxy-2-(4-methoxybenzyl)imino-α-D-glucopyranosyl bromide

There total 3 articles about 3,4,6-tri-O-acetyl-2-deoxy-2-(4-methoxybenzyl)imino-α-D-glucopyranosyl bromide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

(+)-D-glucosamine hydrochloride (1078691-95-8) → 3,4,6-tri-O-acetyl-2-deoxy-2-(4-methoxybenzyl)imino-α-D-glucopyranosyl bromide (61567-93-9)

Guidance literature:

Multi-step reaction with 3 steps

1: sodium hydroxide / methanol; water / Reflux

2: perchloric acid

3: phosphorus; bromine

With phosphorus; perchloric acid; bromine; sodium hydroxide; In methanol; water;

DOI:10.1080/10426507.2011.553208

Reference yield:

4-methoxy-benzaldehyde (123-11-5) → 3,4,6-tri-O-acetyl-2-deoxy-2-(4-methoxybenzyl)imino-α-D-glucopyranosyl bromide (61567-93-9)

Guidance literature:

Multi-step reaction with 3 steps

1: sodium hydroxide / methanol; water / Reflux

2: perchloric acid

3: phosphorus; bromine

With phosphorus; perchloric acid; bromine; sodium hydroxide; In methanol; water;

DOI:10.1080/10426507.2011.553208

Reference yield:

1,3,4,6-tetra-O-acetyl-2-deoxy-2-{[(4-methoxyphenyl)methylidene]amino}-D-glucopyranose (114297-26-6) → 3,4,6-tri-O-acetyl-2-deoxy-2-(4-methoxybenzyl)imino-α-D-glucopyranosyl bromide (61567-93-9)

Guidance literature:

With phosphorus; bromine;

DOI:10.1080/10426507.2011.553208

upstream raw materials:

1,3,4,6-tetra-O-acetyl-2-deoxy-2-{[(4-methoxyphenyl)methylidene]amino}-D-glucopyranose

(+)-D-glucosamine hydrochloride

4-methoxy-benzaldehyde

Downstream raw materials:

methyl 3,4,6-tri-O-acetyl-2-deoxy-2-p-methoxybenzylideneamino-β-D-glucopyranoside

3,4,6-tri-O-acetyl-2-deoxy-2-p-methoxybenzylideneamino-D-glucopyranose

3,4,6-tri-O-acetyl-1,5-anhydro-2-deoxy-2-p-methoxybenzylideneamino-D-arabino-hex-1-enitol

methyl 6-O-(2-acetamido-3,4,6-tri-O-acetyl-2-deoxy-α-D-glucopyranosyl)-2,3,4-tri-O-benzyl-α-D-glucopyranoside

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