tert-butyl 4-({4-[1-(4-chlorophenyl)-1H-pyrazolo[3,4-c]pyridin-3-yl]morpholin-2-yl}methyl)piperazine-1-carboxylate

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Chemical Name:tert-butyl 4-({4-[1-(4-chlorophenyl)-1H-pyrazolo[3,4-c]pyridin-3-yl]morpholin-2-yl}methyl)piperazine-1-carboxylate
CAS No.:1427588-97-3
Molecular Formula:C₂₆H₃₃ClN₆O₃
Molecular Weight:513.039
Hs Code.:

Synonyms:tert-butyl 4-({4-[1-(4-chlorophenyl)-1H-pyrazolo[3,4-c]pyridin-3-yl]morpholin-2-yl}methyl)piperazine-1-carboxylate

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Chemical Property of tert-butyl 4-({4-[1-(4-chlorophenyl)-1H-pyrazolo[3,4-c]pyridin-3-yl]morpholin-2-yl}methyl)piperazine-1-carboxylate

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Technology Process of tert-butyl 4-({4-[1-(4-chlorophenyl)-1H-pyrazolo[3,4-c]pyridin-3-yl]morpholin-2-yl}methyl)piperazine-1-carboxylate

There total 4 articles about tert-butyl 4-({4-[1-(4-chlorophenyl)-1H-pyrazolo[3,4-c]pyridin-3-yl]morpholin-2-yl}methyl)piperazine-1-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 4.0%

: 1427588-95-1
tert-butyl 4-[(4-{1H-pyrazolo[3,4-c]pyridin-3-yl}morpholin-2-yl)methyl]piperazine-1-carboxylate

: 1679-18-1
4-Chlorophenylboronic acid

: 1427588-97-3
tert-butyl 4-({4-[1-(4-chlorophenyl)-1H-pyrazolo[3,4-c]pyridin-3-yl]morpholin-2-yl}methyl)piperazine-1-carboxylate

Guidance literature:: With pyridine; copper diacetate; In 1,2-dichloro-ethane;

Reference yield:

: 55279-29-3
3-amino-pyridine-4-carbaldehyde

: 1427588-97-3
tert-butyl 4-({4-[1-(4-chlorophenyl)-1H-pyrazolo[3,4-c]pyridin-3-yl]morpholin-2-yl}methyl)piperazine-1-carboxylate

Guidance literature:: Multi-step reaction with 3 steps

1: sodium tris(acetoxy)borohydride / dichloromethane / 0.04 h / 60 °C / Microwave irradiation

2: sodium nitrite; acetic acid / water / 0.08 h / 0 °C

3: copper diacetate; pyridine / 1,2-dichloro-ethane

With pyridine; copper diacetate; sodium tris(acetoxy)borohydride; acetic acid; sodium nitrite; In dichloromethane; water; 1,2-dichloro-ethane;

Reference yield:

: 1427588-93-9
tert-butyl 4-({4-[(3-aminopyridin-4-yl)methyl]morpholin-2-yl}methyl)piperazine-1-carboxylate

: 1427588-97-3
tert-butyl 4-({4-[1-(4-chlorophenyl)-1H-pyrazolo[3,4-c]pyridin-3-yl]morpholin-2-yl}methyl)piperazine-1-carboxylate

Guidance literature:: Multi-step reaction with 2 steps

1: sodium nitrite; acetic acid / water / 0.08 h / 0 °C

2: copper diacetate; pyridine / 1,2-dichloro-ethane

With pyridine; copper diacetate; acetic acid; sodium nitrite; In water; 1,2-dichloro-ethane;