6-(5-Acetyl-2-propoxy-phenyl)-1-ethyl-3-methyl-1,5-dihydro-pyrazolo[3,4-d]pyrimidin-4-one

Base Information

Chemical Name:6-(5-Acetyl-2-propoxy-phenyl)-1-ethyl-3-methyl-1,5-dihydro-pyrazolo[3,4-d]pyrimidin-4-one
CAS No.:175406-91-4
Molecular Formula:C₁₉H₂₂N₄O₃
Molecular Weight:354.409
Hs Code.:

Synonyms:6-(5-Acetyl-2-propoxy-phenyl)-1-ethyl-3-methyl-1,5-dihydro-pyrazolo[3,4-d]pyrimidin-4-one

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Chemical Property of 6-(5-Acetyl-2-propoxy-phenyl)-1-ethyl-3-methyl-1,5-dihydro-pyrazolo[3,4-d]pyrimidin-4-one

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Technology Process of 6-(5-Acetyl-2-propoxy-phenyl)-1-ethyl-3-methyl-1,5-dihydro-pyrazolo[3,4-d]pyrimidin-4-one

There total 5 articles about 6-(5-Acetyl-2-propoxy-phenyl)-1-ethyl-3-methyl-1,5-dihydro-pyrazolo[3,4-d]pyrimidin-4-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 506-96-7
Acetyl bromide

: 175406-88-9
1-Ethyl-3-methyl-6-(2-propoxy-phenyl)-1,5-dihydro-pyrazolo[3,4-d]pyrimidin-4-one

: 175406-91-4
6-(5-Acetyl-2-propoxy-phenyl)-1-ethyl-3-methyl-1,5-dihydro-pyrazolo[3,4-d]pyrimidin-4-one

Guidance literature:: With aluminium trichloride; In dichloromethane; for 48h; Ambient temperature;
DOI:10.1021/jm950812j

Reference yield:

: 54090-36-7
2-propoxybenzoyl chloride

: 175406-91-4
6-(5-Acetyl-2-propoxy-phenyl)-1-ethyl-3-methyl-1,5-dihydro-pyrazolo[3,4-d]pyrimidin-4-one

Guidance literature:: Multi-step reaction with 3 steps

1: pyridine / a) RT, b) 45 deg C

2: aq. NaOH, 30percent H₂O₂ / 90 °C

3: 89 percent / AlCl₃ / CH₂Cl₂ / 48 h / Ambient temperature

With pyridine; sodium hydroxide; aluminium trichloride; dihydrogen peroxide; In dichloromethane;
DOI:10.1021/jm950812j

Reference yield:

: 102997-29-5
5-amino-4-cyano-3-methyl-1-ethyl-(1H)-pyrazole

: 175406-91-4
6-(5-Acetyl-2-propoxy-phenyl)-1-ethyl-3-methyl-1,5-dihydro-pyrazolo[3,4-d]pyrimidin-4-one

Guidance literature:: Multi-step reaction with 3 steps

1: pyridine / a) RT, b) 45 deg C

2: aq. NaOH, 30percent H₂O₂ / 90 °C

3: 89 percent / AlCl₃ / CH₂Cl₂ / 48 h / Ambient temperature

With pyridine; sodium hydroxide; aluminium trichloride; dihydrogen peroxide; In dichloromethane;
DOI:10.1021/jm950812j