C₂₂H₂₀Cl₂N₂O₃

Base Information

Chemical Name:C₂₂H₂₀Cl₂N₂O₃
CAS No.:1432059-19-2
Molecular Formula:C₂₂H₂₀Cl₂N₂O₃
Molecular Weight:431.318
Hs Code.:

C<sub>22</sub>H<sub>20</sub>Cl<sub>2</sub>N<sub>2</sub>O<sub>3</sub>

Synonyms:C₂₂H₂₀Cl₂N₂O₃

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₂₂H₂₀Cl₂N₂O₃

Chemical Property:

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Technology Process of C₂₂H₂₀Cl₂N₂O₃

There total 5 articles about C₂₂H₂₀Cl₂N₂O₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

: 945736-71-0
(E)-1-(3-(3,4-dichlorophenyl)allyl)indoline-2,3-dione

: 68014-21-1
triphenyl(t-butoxycarbonylimino)phosphorane

: 1432059-19-2
C₂₂H₂₀Cl₂N₂O₃

Guidance literature:: In 1,4-dioxane; toluene; for 10h; Sealed tube;
DOI:10.1039/c2cc36665g

Reference yield:

: 40950-94-5,82475-77-2
ethyl (E)-3-(3,4-dichloro-phenyl)-2-propenoate

: 1432059-19-2
C₂₂H₂₀Cl₂N₂O₃

Guidance literature:: Multi-step reaction with 4 steps

1.1: diisobutylaluminium hydride / tetrahydrofuran; hexane / 1.17 h / 0 °C / Inert atmosphere

2.1: phosphorus tribromide / diethyl ether / 2 h / 0 °C / Inert atmosphere

3.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 0.5 h / 0 °C / Inert atmosphere

3.2: 1 h / 0 °C / Inert atmosphere

4.1: toluene; 1,4-dioxane / 10 h / Sealed tube

With phosphorus tribromide; sodium hydride; diisobutylaluminium hydride; In tetrahydrofuran; 1,4-dioxane; diethyl ether; hexane; N,N-dimethyl-formamide; toluene; mineral oil; 4.1: |Aza-Wittig Reaction;
DOI:10.1039/c2cc36665g

Reference yield:

: 6287-38-3
3,4-dichlorobenzaldehyde

: 1432059-19-2
C₂₂H₂₀Cl₂N₂O₃

Guidance literature:: Multi-step reaction with 5 steps

1.1: toluene / 6 h / 120 °C / Sealed tube

2.1: diisobutylaluminium hydride / tetrahydrofuran; hexane / 1.17 h / 0 °C / Inert atmosphere

3.1: phosphorus tribromide / diethyl ether / 2 h / 0 °C / Inert atmosphere

4.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 0.5 h / 0 °C / Inert atmosphere

4.2: 1 h / 0 °C / Inert atmosphere

5.1: toluene; 1,4-dioxane / 10 h / Sealed tube

With phosphorus tribromide; sodium hydride; diisobutylaluminium hydride; In tetrahydrofuran; 1,4-dioxane; diethyl ether; hexane; N,N-dimethyl-formamide; toluene; mineral oil; 5.1: |Aza-Wittig Reaction;
DOI:10.1039/c2cc36665g