N-<2-<<(1,1-dimethylethoxy)carbonyl>amino>ethyl>-4-hydroxy-3-nitrobenzenesulfonamide

Base Information

Chemical Name:N-<2-<<(1,1-dimethylethoxy)carbonyl>amino>ethyl>-4-hydroxy-3-nitrobenzenesulfonamide
CAS No.:135685-03-9
Molecular Formula:C₁₃H₁₉N₃O₇S
Molecular Weight:361.376
Hs Code.:

Synonyms:N-<2-<<(1,1-dimethylethoxy)carbonyl>amino>ethyl>-4-hydroxy-3-nitrobenzenesulfonamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-<2-<<(1,1-dimethylethoxy)carbonyl>amino>ethyl>-4-hydroxy-3-nitrobenzenesulfonamide

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Technology Process of N-<2-<<(1,1-dimethylethoxy)carbonyl>amino>ethyl>-4-hydroxy-3-nitrobenzenesulfonamide

There total 3 articles about N-<2-<<(1,1-dimethylethoxy)carbonyl>amino>ethyl>-4-hydroxy-3-nitrobenzenesulfonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 42.0%

: 126813-46-5
N-<2-<<(1-dimethylethoxy)carbonyl>amino>ethyl>-4-chloro-3-nitrobenzenesulfonamide

: 135685-03-9
N-<2-<<(1,1-dimethylethoxy)carbonyl>amino>ethyl>-4-hydroxy-3-nitrobenzenesulfonamide

Guidance literature:: With lithium 2-nitropropane; In dimethyl sulfoxide; for 72h; Ambient temperature;
DOI:10.1021/jm00114a024

Reference yield:

: 57260-73-8
N-BOC-1,2-diaminoethane

: 135685-03-9
N-<2-<<(1,1-dimethylethoxy)carbonyl>amino>ethyl>-4-hydroxy-3-nitrobenzenesulfonamide

Guidance literature:: Multi-step reaction with 2 steps

1: 67.2 percent / N,N-diisopropylethylamine / tetrahydrofuran

2: 42 percent / lithio-2-nitropropane / dimethylsulfoxide / 72 h / Ambient temperature

With lithium 2-nitropropane; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; dimethyl sulfoxide;
DOI:10.1021/jm00114a024

Reference yield:

: 97-08-5
3-nitro-4-chlorosulfonyl chloride

: 135685-03-9
N-<2-<<(1,1-dimethylethoxy)carbonyl>amino>ethyl>-4-hydroxy-3-nitrobenzenesulfonamide

Guidance literature:: Multi-step reaction with 2 steps

1: 67.2 percent / N,N-diisopropylethylamine / tetrahydrofuran

2: 42 percent / lithio-2-nitropropane / dimethylsulfoxide / 72 h / Ambient temperature

With lithium 2-nitropropane; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; dimethyl sulfoxide;
DOI:10.1021/jm00114a024