monophenyl [6-(1,3-dioxo-1,3-dihydroisoindol-2-yl)-1-hydroxy-1-(hydroxy-phenoxy-phosphoryl)hexyl]phosphonate

Base Information

Chemical Name:monophenyl [6-(1,3-dioxo-1,3-dihydroisoindol-2-yl)-1-hydroxy-1-(hydroxy-phenoxy-phosphoryl)hexyl]phosphonate
CAS No.:948317-85-9
Molecular Formula:C₂₆H₂₇NO₉P₂
Molecular Weight:559.449
Hs Code.:

Synonyms:monophenyl [6-(1,3-dioxo-1,3-dihydroisoindol-2-yl)-1-hydroxy-1-(hydroxy-phenoxy-phosphoryl)hexyl]phosphonate

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Chemical Property of monophenyl [6-(1,3-dioxo-1,3-dihydroisoindol-2-yl)-1-hydroxy-1-(hydroxy-phenoxy-phosphoryl)hexyl]phosphonate

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Technology Process of monophenyl [6-(1,3-dioxo-1,3-dihydroisoindol-2-yl)-1-hydroxy-1-(hydroxy-phenoxy-phosphoryl)hexyl]phosphonate

There total 4 articles about monophenyl [6-(1,3-dioxo-1,3-dihydroisoindol-2-yl)-1-hydroxy-1-(hydroxy-phenoxy-phosphoryl)hexyl]phosphonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

: 31968-60-2
6-phthalimidohexanoyl chloride

: 137862-40-9
phenyl bis(trimethylsilyl) phosphite

: 948317-85-9
monophenyl [6-(1,3-dioxo-1,3-dihydroisoindol-2-yl)-1-hydroxy-1-(hydroxy-phenoxy-phosphoryl)hexyl]phosphonate

Guidance literature:: at 20 ℃; for 6h;
DOI:10.1002/ejoc.200601067

Reference yield:

: 85-44-9
phthalic anhydride

: 948317-85-9
monophenyl [6-(1,3-dioxo-1,3-dihydroisoindol-2-yl)-1-hydroxy-1-(hydroxy-phenoxy-phosphoryl)hexyl]phosphonate

Guidance literature:: Multi-step reaction with 3 steps

1: 100 percent / 6 h / 170 °C

2: 100 percent / oxalyl chloride / CH₂Cl₂ / 6 h / Heating

3: 60 percent / 6 h / 20 °C

With oxalyl dichloride; In dichloromethane;
DOI:10.1002/ejoc.200601067

Reference yield:

: 4443-26-9
6-phthalimidohexanoic acid

: 948317-85-9
monophenyl [6-(1,3-dioxo-1,3-dihydroisoindol-2-yl)-1-hydroxy-1-(hydroxy-phenoxy-phosphoryl)hexyl]phosphonate

Guidance literature:: Multi-step reaction with 2 steps

1: 100 percent / oxalyl chloride / CH₂Cl₂ / 6 h / Heating

2: 60 percent / 6 h / 20 °C

With oxalyl dichloride; In dichloromethane;
DOI:10.1002/ejoc.200601067