potassium (3-chloro-2-hydroxyphenyl)trifluoroborate

Base Information

Chemical Name:potassium (3-chloro-2-hydroxyphenyl)trifluoroborate
CAS No.:1033783-04-8
Molecular Formula:C₆H₄BClF₃O*K
Molecular Weight:234.455
Hs Code.:

Synonyms:potassium (3-chloro-2-hydroxyphenyl)trifluoroborate

Suppliers and Price of potassium (3-chloro-2-hydroxyphenyl)trifluoroborate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of potassium (3-chloro-2-hydroxyphenyl)trifluoroborate

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:: SDS file from LookChem

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Technology Process of potassium (3-chloro-2-hydroxyphenyl)trifluoroborate

There total 7 articles about potassium (3-chloro-2-hydroxyphenyl)trifluoroborate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: potassium hydrogen difluoride

: 542-91-6
H₂SiEt₂

: 95-57-8
2-monochlorophenol

: 7732-18-5
water

: 73183-34-3
bis(pinacol)diborane

: 1033783-04-8
potassium (3-chloro-2-hydroxyphenyl)trifluoroborate

Guidance literature:: With pinacol borane; bis(1,5-cyclooctadiene)diiridium(I) dichloride; In tetrahydrofuran; byproducts: H2; ClC6H4OH reacted with (C2H5)2SiH2 and Ir complex in C6H6, reacted with Bcompds., Ir complex and 4,4'-di-tert-butylpyridine in THF at 80° C, reacted with aq. KHF2 in THF;
DOI:10.1021/ja8015878

Reference yield:

: C₁₄H₁₇BClF₆NO₅PS₂

: 1033783-04-8
potassium (3-chloro-2-hydroxyphenyl)trifluoroborate

Guidance literature:: With potassium hydrogen difluoride; In methanol; water; toluene; at 0 - 20 ℃; for 2h; Schlenk technique; Sealed tube; Cooling; Inert atmosphere;
DOI:10.1021/ol303203m