2-(aminocarbonyl)-4-chloro-5-aminobenzaldehyde hydrazone

Base Information

Chemical Name:2-(aminocarbonyl)-4-chloro-5-aminobenzaldehyde hydrazone
CAS No.:100448-58-6
Molecular Formula:C₁₅H₁₂ClF₃N₄O
Molecular Weight:356.735
Hs Code.:

2-(aminocarbonyl)-4-chloro-5-aminobenzaldehyde <m-(trifluoromethyl)phenyl>hydrazone

Synonyms:2-(aminocarbonyl)-4-chloro-5-aminobenzaldehyde hydrazone

Suppliers and Price of 2-(aminocarbonyl)-4-chloro-5-aminobenzaldehyde hydrazone

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Total 1 raw suppliers

Chemical Property of 2-(aminocarbonyl)-4-chloro-5-aminobenzaldehyde hydrazone

Chemical Property:

Purity/Quality:: 99% ，98% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

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Technology Process of 2-(aminocarbonyl)-4-chloro-5-aminobenzaldehyde hydrazone

There total 6 articles about 2-(aminocarbonyl)-4-chloro-5-aminobenzaldehyde hydrazone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 50.0%

: 100448-46-2
5-amino-6-chloro-3-hydroxyphthalimidine

: 368-78-5
3-(trifluoromethyl)phenylhydrazine

: 100448-58-6
2-(aminocarbonyl)-4-chloro-5-aminobenzaldehyde hydrazone

Guidance literature:: In ethanol; water; at 95 ℃; for 12h;
DOI:10.1021/jm00156a011

Reference yield:

: 7147-90-2
4-chlorophthalimide

: 100448-58-6
2-(aminocarbonyl)-4-chloro-5-aminobenzaldehyde hydrazone

Guidance literature:: Multi-step reaction with 4 steps

1: 66 percent / 20percent oleum, fuming nitric acid / 0.5 h / 80 °C

2: 80 percent / SnCl₂*2H₂O, concd. HCl / 0.5 h / 60 °C

3: 61 percent / Zn, CuSO₄*5H₂O, 2 N NaOH

4: 50 percent / H₂O; ethanol / 12 h / 95 °C

With hydrogenchloride; sodium hydroxide; sulfuric acid; nitric acid; copper(II) sulfate; tin(ll) chloride; zinc; In ethanol; water;
DOI:10.1021/jm00156a011

Reference yield:

: 6015-57-2
5-chloro-6-nitroisoindole-1,3-dione

: 100448-58-6
2-(aminocarbonyl)-4-chloro-5-aminobenzaldehyde hydrazone

Guidance literature:: Multi-step reaction with 3 steps

1: 80 percent / SnCl₂*2H₂O, concd. HCl / 0.5 h / 60 °C

2: 61 percent / Zn, CuSO₄*5H₂O, 2 N NaOH

3: 50 percent / H₂O; ethanol / 12 h / 95 °C

With hydrogenchloride; sodium hydroxide; copper(II) sulfate; tin(ll) chloride; zinc; In ethanol; water;
DOI:10.1021/jm00156a011