2,4-di-phenyl-6-(pyridin-3-yl)-1,3,5-triazine

Base Information

• Chemical Name: 2,4-di-phenyl-6-(pyridin-3-yl)-1,3,5-triazine
• CAS No.: 1596320-79-4
• Molecular Formula: C₂₀H₁₄N₄
• Molecular Weight: 310.358
• Mol file: 1596320-79-4.mol

Synonyms:2,4-di-phenyl-6-(pyridin-3-yl)-1,3,5-triazine

Chemical Property of 2,4-di-phenyl-6-(pyridin-3-yl)-1,3,5-triazine

Chemical Property:

Purity/Quality:

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MSDS Files:

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Technology Process of 2,4-di-phenyl-6-(pyridin-3-yl)-1,3,5-triazine

There total 3 articles about 2,4-di-phenyl-6-(pyridin-3-yl)-1,3,5-triazine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

3-hydroxymethylpyridin (100-55-0) + benzamidine monohydrochloride (1670-14-0) → 2,4-di-phenyl-6-(pyridin-3-yl)-1,3,5-triazine (1596320-79-4)

Guidance literature:

With oxygen; copper(II) acetate monohydrate; sodium carbonate; In toluene; at 110 ℃; for 24h;

DOI:10.1039/c5ob00724k

Reference yield: 96.0%

3-Aminomethylpyridine (3731-52-0) + benzamidine monohydrochloride (1670-14-0) → 2,4-di-phenyl-6-(pyridin-3-yl)-1,3,5-triazine (1596320-79-4)

Guidance literature:

With oxygen; caesium carbonate; at 130 ℃; for 3h; Green chemistry;

DOI:10.1039/c5gc01884f

Reference yield: 85.0%

methyl-3-pyridylketone (350-03-8) + benzamidine monohydrochloride (1670-14-0) → 2,4-di-phenyl-6-(pyridin-3-yl)-1,3,5-triazine (1596320-79-4)

Guidance literature:

With iodine; caesium carbonate; In dimethyl sulfoxide; at 20 - 110 ℃; for 16.0833h; regioselective reaction;

DOI:10.1021/acs.joc.7b02313

upstream raw materials:

3-hydroxymethylpyridin

benzamidine monohydrochloride

3-Aminomethylpyridine

methyl-3-pyridylketone