(S)-(3,3-dimethyl-2,4-bis(3-methylbut-2-enyl)cyclohex-1-enyloxy)trimethylsilane

Base Information

Chemical Name:(S)-(3,3-dimethyl-2,4-bis(3-methylbut-2-enyl)cyclohex-1-enyloxy)trimethylsilane
CAS No.:1256246-05-5
Molecular Formula:C₂₁H₃₈OSi
Molecular Weight:334.618
Hs Code.:

Synonyms:(S)-(3,3-dimethyl-2,4-bis(3-methylbut-2-enyl)cyclohex-1-enyloxy)trimethylsilane

Suppliers and Price of (S)-(3,3-dimethyl-2,4-bis(3-methylbut-2-enyl)cyclohex-1-enyloxy)trimethylsilane

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (S)-(3,3-dimethyl-2,4-bis(3-methylbut-2-enyl)cyclohex-1-enyloxy)trimethylsilane

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Technology Process of (S)-(3,3-dimethyl-2,4-bis(3-methylbut-2-enyl)cyclohex-1-enyloxy)trimethylsilane

There total 1 articles about (S)-(3,3-dimethyl-2,4-bis(3-methylbut-2-enyl)cyclohex-1-enyloxy)trimethylsilane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 75-77-4
chloro-trimethyl-silane

: 1256246-04-4
(S)-3-methyl-2,4-bis(3-methylbut-2-enyl)cyclohex-2-enone

: 75-16-1
methylmagnesium bromide

: 1256246-05-5
(S)-(3,3-dimethyl-2,4-bis(3-methylbut-2-enyl)cyclohex-1-enyloxy)trimethylsilane

Guidance literature:: With copper(I) bromide dimethylsulfide complex; In tetrahydrofuran; N,N,N,N,N,N-hexamethylphosphoric triamide; diethyl ether; at -78 - -40 ℃; for 4h; Inert atmosphere;
DOI:10.1021/ol1022728

Reference yield:

: 1256246-05-5
(S)-(3,3-dimethyl-2,4-bis(3-methylbut-2-enyl)cyclohex-1-enyloxy)trimethylsilane

: 1256246-06-6
(4S)-3,3-dimethyl-2,4-bis(3-methylbut-2-enyl)cyclohexanone

Guidance literature:: With hydrogenchloride; water; In tetrahydrofuran; N,N,N,N,N,N-hexamethylphosphoric triamide; diethyl ether; for 0.0833333h; optical yield given as %de; Inert atmosphere;
DOI:10.1021/ol1022728