phenyl 1-(triphenylsilyl)vinyl ketone

Base Information

Chemical Name:phenyl 1-(triphenylsilyl)vinyl ketone
CAS No.:49750-05-2
Molecular Formula:C₂₇H₂₂OSi
Molecular Weight:390.557
Hs Code.:

Synonyms:phenyl 1-(triphenylsilyl)vinyl ketone

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Chemical Property of phenyl 1-(triphenylsilyl)vinyl ketone

Chemical Property:

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Technology Process of phenyl 1-(triphenylsilyl)vinyl ketone

There total 2 articles about phenyl 1-(triphenylsilyl)vinyl ketone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 18676-45-4
α-bromovinyltriphenylsilane

: 93-97-0
benzoic acid anhydride

: 49750-05-2
phenyl 1-(triphenylsilyl)vinyl ketone

Guidance literature:: Multistep reaction; (i) nBuLi, (ii) /BRN= 516726/;
DOI:10.1139/v73-302

Reference yield:

: 52629-60-4
1-phenyl-2-triphenylsilyl-2-propen-1-ol

: 49750-05-2
phenyl 1-(triphenylsilyl)vinyl ketone

Guidance literature:: DOI:10.1002/anie.201003152

Reference yield: 79.0%

: C₄H₉O^(1-)*C₆H₅Cu*Cu⁽¹⁺⁾

: 49750-05-2
phenyl 1-(triphenylsilyl)vinyl ketone

: 563-47-3
3-Chloro-2-methylpropene

: 1256237-15-6
(1E)-2-benzyl-4-methyl-1-phenyl-1-(triphenylsiloxy)-1,4-pentadiene

Guidance literature:: C₄H₉O^(1-)*C₆H₅Cu*Cu⁽¹⁺⁾; phenyl 1-(triphenylsilyl)vinyl ketone; In tetrahydrofuran; at 0 ℃; for 2h;

With N,N-dimethyl-formamide; In tetrahydrofuran; at 50 ℃; for 0.5h;

3-Chloro-2-methylpropene; In tetrahydrofuran; N,N-dimethyl-formamide; at 50 ℃; for 4h; stereoselective reaction;
DOI:10.1002/anie.201003152