C₁₂H₉ClN₂O₃

Base Information

Chemical Name:C₁₂H₉ClN₂O₃
CAS No.:1426320-73-1
Molecular Formula:C₁₂H₉ClN₂O₃
Molecular Weight:264.668
Hs Code.:

C<sub>12</sub>H<sub>9</sub>ClN<sub>2</sub>O<sub>3</sub>

Synonyms:C₁₂H₉ClN₂O₃

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Chemical Property of C₁₂H₉ClN₂O₃

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Technology Process of C₁₂H₉ClN₂O₃

There total 5 articles about C₁₂H₉ClN₂O₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 67-56-1
methanol

: 1426320-72-0
C₁₁H₇ClN₂O₃

: 1426320-73-1
C₁₂H₉ClN₂O₃

Guidance literature:: With sulfuric acid; for 4h; Reflux;

Reference yield:

: 1426320-70-8
C₁₁H₈Cl₂N₂O

: 1426320-73-1
C₁₂H₉ClN₂O₃

Guidance literature:: Multi-step reaction with 3 steps

1: dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂; triethylamine / 16 h / 50 °C / 3750.38 Torr / Inert atmosphere

2: boron tribromide / dichloromethane / -78 - 20 °C / Inert atmosphere

3: sulfuric acid / 4 h / Reflux

With dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂; sulfuric acid; boron tribromide; triethylamine; In dichloromethane;

Reference yield:

: 16817-43-9
5-Bromo-2-chloroanisole

: 1426320-73-1
C₁₂H₉ClN₂O₃

Guidance literature:: Multi-step reaction with 5 steps

1.1: n-butyllithium / tetrahydrofuran; toluene / 0.5 h / -78 °C / Inert atmosphere

1.2: 16 h / 20 °C

2.1: tetrakis(triphenylphosphine) palladium⁽⁰⁾; potassium carbonate / 1,4-dioxane / 3 h / 90 °C / Inert atmosphere

3.1: dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂; triethylamine / 16 h / 50 °C / 3750.38 Torr / Inert atmosphere

4.1: boron tribromide / dichloromethane / -78 - 20 °C / Inert atmosphere

5.1: sulfuric acid / 4 h / Reflux

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; n-butyllithium; dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂; sulfuric acid; boron tribromide; potassium carbonate; triethylamine; In tetrahydrofuran; 1,4-dioxane; dichloromethane; toluene;