dimethyl 3,3'-[4-(4-chlorophenyl)pyridine-2,6-diyl]dipropanoate

Base Information

Chemical Name:dimethyl 3,3'-[4-(4-chlorophenyl)pyridine-2,6-diyl]dipropanoate
CAS No.:1364054-49-8
Molecular Formula:C₁₉H₂₀ClNO₄
Molecular Weight:361.825
Hs Code.:

Synonyms:dimethyl 3,3'-[4-(4-chlorophenyl)pyridine-2,6-diyl]dipropanoate

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Chemical Property of dimethyl 3,3'-[4-(4-chlorophenyl)pyridine-2,6-diyl]dipropanoate

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Technology Process of dimethyl 3,3'-[4-(4-chlorophenyl)pyridine-2,6-diyl]dipropanoate

There total 4 articles about dimethyl 3,3'-[4-(4-chlorophenyl)pyridine-2,6-diyl]dipropanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 1364054-33-0
dimethyl (2E,2'E)-3,3'-[4-(4-chlorophenyl)pyridine-2,6-diyl]bisprop-2-enoate

: 1364054-49-8
dimethyl 3,3'-[4-(4-chlorophenyl)pyridine-2,6-diyl]dipropanoate

Guidance literature:: With palladium on activated charcoal; hydrogen; In methanol; at 60 ℃; for 15h; under 760.051 Torr;
DOI:10.1002/hlca.201100195

Reference yield: 84.0%

: 1364054-36-3
dimethyl 3,3'-(4-bromopyridine-2,6-diyl)dipropanoate

: 1679-18-1
4-Chlorophenylboronic acid

: 1364054-49-8
dimethyl 3,3'-[4-(4-chlorophenyl)pyridine-2,6-diyl]dipropanoate

Guidance literature:: With potassium fluoride; potassium carbonate; triphenylphosphine; In 1,2-dimethoxyethane; water; at 95 ℃; for 48h;
DOI:10.1002/hlca.201100195

Reference yield:

: 1364054-24-9
dimethyl (2E,2'E)-3,3'-(4-bromopyridine-2,6-diyl)bisprop-2-enoate

: 1364054-49-8
dimethyl 3,3'-[4-(4-chlorophenyl)pyridine-2,6-diyl]dipropanoate

Guidance literature:: Multi-step reaction with 2 steps

1: sodium tetrahydroborate; hydrogen; nickel diacetate / methanol; ethyl acetate / 0.25 h / 20 °C / 760.05 Torr

2: potassium fluoride; potassium carbonate; triphenylphosphine / 1,2-dimethoxyethane; water / 48 h / 95 °C

With potassium fluoride; sodium tetrahydroborate; hydrogen; nickel diacetate; potassium carbonate; triphenylphosphine; In methanol; 1,2-dimethoxyethane; water; ethyl acetate; 2: Suzuki coupling;
DOI:10.1002/hlca.201100195