1-(4-Fluorphenyl)-2-phenyl-1-ethanon-p-tolylsulfonylhydrazon

Base Information

• Chemical Name: 1-(4-Fluorphenyl)-2-phenyl-1-ethanon-p-tolylsulfonylhydrazon
• CAS No.: 73424-43-8
• Molecular Formula: C₂₁H₁₉FN₂O₂S
• Molecular Weight: 382.458
• Mol file: 73424-43-8.mol

Synonyms:1-(4-Fluorphenyl)-2-phenyl-1-ethanon-p-tolylsulfonylhydrazon

Chemical Property of 1-(4-Fluorphenyl)-2-phenyl-1-ethanon-p-tolylsulfonylhydrazon

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

Useful:

Technology Process of 1-(4-Fluorphenyl)-2-phenyl-1-ethanon-p-tolylsulfonylhydrazon

There total 3 articles about 1-(4-Fluorphenyl)-2-phenyl-1-ethanon-p-tolylsulfonylhydrazon which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 77.0%

1-(4-fluorophenyl)-2-phenylethanone (347-84-2) + toluene-4-sulfonic acid hydrazide (1576-35-8) → 1-(4-Fluorphenyl)-2-phenyl-1-ethanon-p-tolylsulfonylhydrazon (73424-43-8)

Guidance literature:

In ethanol; for 3h; Heating;

Reference yield:

fluorobenzene (462-06-6) → 1-(4-Fluorphenyl)-2-phenyl-1-ethanon-p-tolylsulfonylhydrazon (73424-43-8)

Guidance literature:

Multi-step reaction with 2 steps

1: 36 percent / AlCl₃ / 1) 30 deg C, 2 h, 2) 50-60 deg C, 3 h

2: 77 percent / ethanol / 3 h / Heating

With aluminium trichloride; In ethanol;

Reference yield:

phenylacetyl chloride (103-80-0) → 1-(4-Fluorphenyl)-2-phenyl-1-ethanon-p-tolylsulfonylhydrazon (73424-43-8)

Guidance literature:

Multi-step reaction with 2 steps

1: 36 percent / AlCl₃ / 1) 30 deg C, 2 h, 2) 50-60 deg C, 3 h

2: 77 percent / ethanol / 3 h / Heating

With aluminium trichloride; In ethanol;

upstream raw materials:

1-(4-fluorophenyl)-2-phenylethanone

toluene-4-sulfonic acid hydrazide

fluorobenzene

phenylacetyl chloride

Downstream raw materials:

4-(4-Fluorphenyl)-5-phenyl-1,2,3-thiadiazol