2--1,3-dichloro-2-propanol

Base Information

Chemical Name:2--1,3-dichloro-2-propanol
CAS No.:106418-66-0
Molecular Formula:C₁₉H₃₀Cl₂O
Molecular Weight:345.353
Hs Code.:

2-<p-(n-decyl)phenyl>-1,3-dichloro-2-propanol

Synonyms:2--1,3-dichloro-2-propanol

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2--1,3-dichloro-2-propanol

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Technology Process of 2--1,3-dichloro-2-propanol

There total 3 articles about 2--1,3-dichloro-2-propanol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 37529-30-9
4-n-decylaniline

: 106418-66-0
2--1,3-dichloro-2-propanol

Guidance literature:: Multi-step reaction with 3 steps

1: 1.) 3 N aq. HCl, sodium nitrite, 2.) 48percent aq. fluoroboric acid / 1.) 0-5 deg C, 2.) 20 min

2: 61 percent / bromotrichloromethane, KOAc, 18-crown-6 / tetrahydrofuran / 3 h / Ambient temperature

3: 1.) Mg, I₂ / 1.) Et₂O, RT, 2.) Et₂O, -60 deg C, 0.5 h

With hydrogenchloride; tetrafluoroboric acid; 18-crown-6 ether; Bromotrichloromethane; iodine; potassium acetate; magnesium; sodium nitrite; In tetrahydrofuran;
DOI:10.1021/jo00380a012

Reference yield:

: 4-n-decylbenzenediazonium tetrafluoroborate

: 106418-66-0
2--1,3-dichloro-2-propanol

Guidance literature:: Multi-step reaction with 2 steps

1: 61 percent / bromotrichloromethane, KOAc, 18-crown-6 / tetrahydrofuran / 3 h / Ambient temperature

2: 1.) Mg, I₂ / 1.) Et₂O, RT, 2.) Et₂O, -60 deg C, 0.5 h

With 18-crown-6 ether; Bromotrichloromethane; iodine; potassium acetate; magnesium; In tetrahydrofuran;
DOI:10.1021/jo00380a012

Reference yield:

: 106418-67-1
1-bromo-4-n-decyl benzene

: 534-07-6
1,3-Dichloroacetone

: 106418-66-0
2--1,3-dichloro-2-propanol

Guidance literature:: With iodine; magnesium; Yield given. Multistep reaction; 1.) Et₂O, RT, 2.) Et₂O, -60 deg C, 0.5 h;
DOI:10.1021/jo00380a012