N-allyl-N-benzylbenzamide

Base Information

Chemical Name:N-allyl-N-benzylbenzamide
CAS No.:210347-84-5
Molecular Formula:C₁₇H₁₇NO
Molecular Weight:251.328
Hs Code.:

Synonyms:N-allyl-N-benzylbenzamide

Suppliers and Price of N-allyl-N-benzylbenzamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-allyl-N-benzylbenzamide

Chemical Property:

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Technology Process of N-allyl-N-benzylbenzamide

There total 4 articles about N-allyl-N-benzylbenzamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 59.0%

: 591-87-7
Allyl acetate

: 1485-70-7
N-benzylbenzamide

: 210347-84-5
N-allyl-N-benzylbenzamide

Guidance literature:: N-benzylbenzamide; With sodium hydride; In tetrahydrofuran; mineral oil; at 20 ℃; for 1h;

Allyl acetate; With allyl(cyclopentadiene)palladium(II); tris(para-trifluoromethyl)phenyl phosphine; In tetrahydrofuran; mineral oil; at 50 ℃; for 24h;
DOI:10.1039/c0cc05308b

Reference yield:

: 98-88-4
benzoyl chloride

: 210347-84-5
N-allyl-N-benzylbenzamide

Guidance literature:: Multi-step reaction with 2 steps

1.1: triethylamine / dichloromethane / 0 - 20 °C / Inert atmosphere

2.1: sodium hydride / 0.5 h / 0 - 50 °C

2.2: 0 - 50 °C

With sodium hydride; triethylamine; In dichloromethane;
DOI:10.1002/anie.202009115