PdPtCo₂(CO)7(dppm)2

Base Information

Chemical Name:PdPtCo₂(CO)7(dppm)2
CAS No.:113109-37-8
Molecular Formula:C₅₇H₄₄Co₂O₇P₄PdPt
Molecular Weight:1384.35
Hs Code.:

Synonyms:PdPtCo₂(CO)7(dppm)2

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Chemical Property of PdPtCo₂(CO)7(dppm)2

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Technology Process of PdPtCo₂(CO)7(dppm)2

There total 4 articles about PdPtCo₂(CO)7(dppm)2 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 14878-28-5
sodium tetracarbonyl cobaltate

: 82307-36-6
{PdPtCl₂(dppm)2}

: 113109-37-8
PdPtCo₂(CO)7(dppm)2

Guidance literature:: In tetrahydrofuran; byproducts: NaCl; A filtered soln. of Na{Co(CO)4} in THF was added to cooled (0°C) and stirred susp. of {PdPtCl2(dppm)2} in THF. Stirred for 3 h.; The soln. was concd. in vac. and filtered to remove NaCl. Addn. of pentane gave, after cooling at -20°C, a quant. yield of a mikrocrystalline powder, which was washed with water and dried in vac. Elem.anal.;

Reference yield: 80.0%

: 14878-28-5
sodium tetracarbonyl cobaltate

: 82307-38-8
{PdPtI₂(dppm)2}

: 113109-37-8
PdPtCo₂(CO)7(dppm)2

Guidance literature:: In chloroform-d1; A filtered soln. of Na{Co(CO)4} in THF was added to a cooled (0°C) and stirred susp. of {PdPtI2(dppm)2} in CDCl3.; Identified by 31P-NMR. Further unidentified products. When the solvent was removed in vac., the resulting solid was red. Extn. with toluene gave a green soln. of PdPtCo2(CO)7(dppm)2.;

Reference yield: 54.0%

: 14878-28-5
sodium tetracarbonyl cobaltate

: 82307-36-6
{PdPtCl₂(dppm)2}

: 14362-44-8,20461-54-5,69239-56-1
iodide

: 113109-37-8
PdPtCo₂(CO)7(dppm)2

: 82307-38-8
{PdPtI₂(dppm)2}

: 16887-00-6
chloride

Guidance literature:: In tetrahydrofuran; A THF soln. of Na{Co(CO)4} was added at 0°C to a mixt. of {PdPtCl2(dppm)2} and I(1-) in THF. After 2 h of react. at 0°C and 2 h of react. at room temp., the pale yellow soln. had turned brown-red.; Filtration and crystn. in THF/Et2O afforded a powder. The IR spectrum (in THF) of the green mother liquor revealed exclusively the presence of PdPtCo2(CO)7(dppm)2.;