tributyl-[5-(3,5-dichloro-phenyl)-5-trifluoromethyl-2,5-dihydro-furan-3-yl]-stannane

Base Information

Chemical Name:tributyl-[5-(3,5-dichloro-phenyl)-5-trifluoromethyl-2,5-dihydro-furan-3-yl]-stannane
CAS No.:1331886-76-0
Molecular Formula:C₂₃H₃₃Cl₂F₃OSn
Molecular Weight:572.126
Hs Code.:

Synonyms:tributyl-[5-(3,5-dichloro-phenyl)-5-trifluoromethyl-2,5-dihydro-furan-3-yl]-stannane

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of tributyl-[5-(3,5-dichloro-phenyl)-5-trifluoromethyl-2,5-dihydro-furan-3-yl]-stannane

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Technology Process of tributyl-[5-(3,5-dichloro-phenyl)-5-trifluoromethyl-2,5-dihydro-furan-3-yl]-stannane

There total 4 articles about tributyl-[5-(3,5-dichloro-phenyl)-5-trifluoromethyl-2,5-dihydro-furan-3-yl]-stannane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1331887-03-6
C₂₃H₃₅Cl₂F₃O₂Sn

: 1331886-76-0
tributyl-[5-(3,5-dichloro-phenyl)-5-trifluoromethyl-2,5-dihydro-furan-3-yl]-stannane

Guidance literature:: With triphenylphosphine; diethylazodicarboxylate; In tetrahydrofuran; at 0 ℃; for 1.5h; Inert atmosphere;

Reference yield:

: 1331887-02-5
C₁₄H₁₅Cl₂F₃O₂Si

: 1331886-76-0
tributyl-[5-(3,5-dichloro-phenyl)-5-trifluoromethyl-2,5-dihydro-furan-3-yl]-stannane

Guidance literature:: Multi-step reaction with 3 steps

1: tetrabutyl ammonium fluoride / ethyl acetate; tetrahydrofuran / 22 h / Inert atmosphere

2: tetrakis(triphenylphosphine) palladium⁽⁰⁾ / toluene / 0.75 h / Inert atmosphere

3: triphenylphosphine; diethylazodicarboxylate / tetrahydrofuran / 1.5 h / 0 °C / Inert atmosphere

With tetrabutyl ammonium fluoride; triphenylphosphine; diethylazodicarboxylate; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In tetrahydrofuran; ethyl acetate; toluene;

Reference yield:

: 1331886-75-9
4-(3,5-dichloro-phenyl)-5,5,5-trifluoro-pent-2-yne-1,4-diol

: 1331886-76-0
tributyl-[5-(3,5-dichloro-phenyl)-5-trifluoromethyl-2,5-dihydro-furan-3-yl]-stannane

Guidance literature:: Multi-step reaction with 2 steps

1: tetrakis(triphenylphosphine) palladium⁽⁰⁾ / toluene / 0.75 h / Inert atmosphere

2: triphenylphosphine; diethylazodicarboxylate / tetrahydrofuran / 1.5 h / 0 °C / Inert atmosphere

With triphenylphosphine; diethylazodicarboxylate; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In tetrahydrofuran; toluene;