isopropyl (R)-(+)-2-acetoxy-5-[4-[2-(2-furyl)-5-methyl-4-oxazolylmethoxy]-3-methoxyphenyl]valerate

Base Information

Chemical Name:isopropyl (R)-(+)-2-acetoxy-5-[4-[2-(2-furyl)-5-methyl-4-oxazolylmethoxy]-3-methoxyphenyl]valerate
CAS No.:178610-78-1
Molecular Formula:C₂₆H₃₁NO₈
Molecular Weight:485.534
Hs Code.:

Synonyms:isopropyl (R)-(+)-2-acetoxy-5-[4-[2-(2-furyl)-5-methyl-4-oxazolylmethoxy]-3-methoxyphenyl]valerate

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Chemical Property of isopropyl (R)-(+)-2-acetoxy-5-[4-[2-(2-furyl)-5-methyl-4-oxazolylmethoxy]-3-methoxyphenyl]valerate

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Technology Process of isopropyl (R)-(+)-2-acetoxy-5-[4-[2-(2-furyl)-5-methyl-4-oxazolylmethoxy]-3-methoxyphenyl]valerate

There total 1 articles about isopropyl (R)-(+)-2-acetoxy-5-[4-[2-(2-furyl)-5-methyl-4-oxazolylmethoxy]-3-methoxyphenyl]valerate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 44.0%

: 108-05-4,9003-20-7
vinyl acetate

: 178610-77-0
isopropyl 5-[4-[2-(2-furyl)-5-methyl-4-oxazolylmethoxy]-3-methoxyphenyl]-2-hydroxyvalerate

: 178610-79-2
isopropyl (S)-(-)-5-[4-[2-(2-furyl)-5-methyl-4-oxazolylmethoxy]-3-methoxyphenyl]-2-hydroxyvalerate

: 178610-78-1
isopropyl (R)-(+)-2-acetoxy-5-[4-[2-(2-furyl)-5-methyl-4-oxazolylmethoxy]-3-methoxyphenyl]valerate

Guidance literature:: With immobilized lipase from Pseudomonas sp; In toluene; at 23 ℃; for 4h;
DOI:10.1021/jm010490l

Reference yield: 77.0%

: 67-56-1
methanol

: 178610-78-1
isopropyl (R)-(+)-2-acetoxy-5-[4-[2-(2-furyl)-5-methyl-4-oxazolylmethoxy]-3-methoxyphenyl]valerate

: 178610-81-6
methyl (R)-5-[4-[2-(2-furyl)-5-methyl-4-oxazolylmethoxy]-3-methoxyphenyl]-2-hydroxyvalerate

Guidance literature:: With hydrogenchloride; at 20 ℃; for 12h;
DOI:10.1021/jm010490l

Reference yield:

: 178610-78-1
isopropyl (R)-(+)-2-acetoxy-5-[4-[2-(2-furyl)-5-methyl-4-oxazolylmethoxy]-3-methoxyphenyl]valerate

: 178610-85-0
methyl (R)-(+)-2-carbamoyloxy-5-[4-[2-(2-furyl)-5-methyl-4-oxazolylmethoxy]-3-methoxyphenyl]valerate

Guidance literature:: Multi-step reaction with 3 steps

1: 77 percent / HCl / 12 h / 20 °C

2: 98 percent / pyridine / 1 h / 20 °C

3: 89 percent / NH₃ / tetrahydrofuran / 0.17 h / -65 °C

With pyridine; hydrogenchloride; ammonia; In tetrahydrofuran;
DOI:10.1021/jm010490l