6-(4-fluorophenyl)-4-imino-7-phenylpyrrolo[2,3-d][1,3]thiazin-2(1H,4H,7H)-thione

Base Information

• Chemical Name: 6-(4-fluorophenyl)-4-imino-7-phenylpyrrolo[2,3-d][1,3]thiazin-2(1H,4H,7H)-thione
• CAS No.: 1605289-01-7
• Molecular Formula: C₁₈H₁₂FN₃S₂
• Molecular Weight: 353.444

Synonyms:6-(4-fluorophenyl)-4-imino-7-phenylpyrrolo[2,3-d][1,3]thiazin-2(1H,4H,7H)-thione

Chemical Property of 6-(4-fluorophenyl)-4-imino-7-phenylpyrrolo[2,3-d][1,3]thiazin-2(1H,4H,7H)-thione

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Technology Process of 6-(4-fluorophenyl)-4-imino-7-phenylpyrrolo[2,3-d][1,3]thiazin-2(1H,4H,7H)-thione

There total 1 articles about 6-(4-fluorophenyl)-4-imino-7-phenylpyrrolo[2,3-d][1,3]thiazin-2(1H,4H,7H)-thione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

carbon disulfide (75-15-0,12122-00-8) + 2-amino-5-(4-fluoro-phenyl)-1-phenyl-1H-pyrrole-3-carbonitrile (748810-21-1) → 6-(4-fluorophenyl)-4-imino-7-phenylpyrrolo[2,3-d][1,3]thiazin-2(1H,4H,7H)-thione (1605289-01-7)

Guidance literature:

With pyridine; for 3h; Reflux;

DOI:10.1016/j.ejmech.2014.03.068

Reference yield: 85.0%

6-(4-fluorophenyl)-4-imino-7-phenylpyrrolo[2,3-d][1,3]thiazin-2(1H,4H,7H)-thione (1605289-01-7) + ethyl iodide (75-03-6) → 2-(ethylthio)-6-(4-fluorophenyl)-7-phenylpyrrolo[2,3-d][1,3]thiazin-4(7H)-imine (1605289-06-2)

Guidance literature:

With sodium hydride; In N,N-dimethyl-formamide; for 24h;

DOI:10.1016/j.ejmech.2014.03.068

Reference yield: 85.0%

6-(4-fluorophenyl)-4-imino-7-phenylpyrrolo[2,3-d][1,3]thiazin-2(1H,4H,7H)-thione (1605289-01-7) + s-butyl bromide (78-76-2,5787-31-5) → 2-(sec-butylthio)-6-(4-fluorophenyl)-7-phenylpyrrolo[2,3-d][1,3]thiazin-4(7H)-imine (1605289-11-9)

Guidance literature:

With sodium hydride; In N,N-dimethyl-formamide; for 24h;

DOI:10.1016/j.ejmech.2014.03.068

upstream raw materials:

carbon disulfide

2-amino-5-(4-fluoro-phenyl)-1-phenyl-1H-pyrrole-3-carbonitrile

Downstream raw materials:

6-(4-fluorophenyl)-7-phenyl-1H-pyrrolo[2,3-d]pyrimidine-2,4(3H,7H)-dithione

3-amino-6-(4-fluorophenyl)-4-imino-7-phenyl-1,3,4,7-tetrahydro-2H-pyrrolo[2,3-d]pyrimidine-2-thione

2-(ethylthio)-6-(4-fluorophenyl)-7-phenylpyrrolo[2,3-d][1,3]thiazin-4(7H)-imine

2-(sec-butylthio)-6-(4-fluorophenyl)-7-phenylpyrrolo[2,3-d][1,3]thiazin-4(7H)-imine

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